GCMS analysis results for sample AE00110, Feb 2002

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Data File : C: \MSDCHEM\1\5973N\02FEB04\00110 . D vial: 4 . Acq On 4 Feb 2002 1:28 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 4, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 2 N,N’ -Diacetylethylenediamin... Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 4.24 0.12 ug/L 61987 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 N,N’ -Diacetylethylenediamine $$ ... 144 C6H12N202 000871-78-3 33 2 Isothiazole 85 C3H3NS 000288-16-4 9 3 Morpholine $$ p-Isoxazine, tetra... 87 C4H9NO 000110-91-8 9 4 Isothiazole (CAS) $$ 1,2-THIAZOLE 85 C3H3NS 000288-16-4 9 Abundance Scan 76 (4.241 min): 00110.D (-) m/ z 85.00 100.00% 85 41

5000

55 60 89 AMA 3.80 4.00 4.20 4.40 4.60 ‘ m/z—> 5 0b11n-19010—03uETT 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 ,4910—* TPTRTPp i • “ ■ i ■ • m/z 41.10 80.39% Abundance #39767: N,N’-Diacetylethylenediamine $$ Acetamide, N,N'-1,... 43 30

5000 73 85 ■ . A NAAY i • ‘ 1 •i ■ * ■ ‘ i * • • ‘ i 3.80 4.00 4.20 4.40 4.60 m/z 43.10 66.69%

miz-> Abundance 5 0b 15

’ ’’1’14’153 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 zGl,. #3569: Isothiazole Hmm 85 AAA 3.80 4.00 4.20 4.40 4.60 5000 58 m/z 87.10 33.42%

39 45 52 On1 .. , । . , . . । . 1,. ।. .,, j ■, , ,, > ... । . . , I! . . . I [. , i 1 | 1 1 , TTWITTTTTTTT /z—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #4374: Morpholine $$ p-Isoxazine, tetrahydro- $$ BASF 238 ... 23 57 3.80 4.00 4.20 4.40 4.60 m/z 39.10 29.67% 5000 87

42 54 0b. t.. t >. > > (.... ।....!. 1 “1 ’17 THH ''in -- vfz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 3.80 4.00 4.20 4.40 4.60

)0110.D SCAN508.M Tue Feb 05 09:47:01 2002 Page 4

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