GCMS results for sample AE00463, Jan 24 2002

NYC 9/11 Public Portal Document

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Data File : C:\MSDCHEM\1\5973N\02JAN11\00463.D Vial: 5 Acq On : 11 Jan 2002 5:25 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 11, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L

Peak Number 2 3-Buten-2-ol, 2-methyl- Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 5.01 0.36 ug/L 110595 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2 3 3-Buten-2-ol, 2-methyl- 3-Buten-2-ol, 2-methyl- 3-Buten-2-ol, 2-methyl- C

(N Up 86 C5H10O 86 C5H10O 86 C5H10O 000115-18-4 000115-18-4 000115-18-4 90 80 78 4 Butenol, methyl-_________________ 86 C5H10O 060766-00-9 72 Abundance Scan 143 (5.006 min): 00463.D (-) m/z 71.10 100.00% 43 71

5000 59 39 55 AA ) 1118’" i ■ ‘ ‘It’E । r' ' 86 67 4 60 4.80 5.00 5.20 5.40 OPP . + J- 11 m > 11 + — hij...... THTTTPPPT m/z 43.10 86.82% mz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #4085: 3-Buten-2-ol, 2-methyl- 71 43

5000 59 ATM A , 4.60 4.80 5.00 h 5.20© 5.40/ 27 31 m/ z 41.10 65.32% 53

mlz-> 0 ■ ■ i • ■. ■ । ■ 20 25 30 11I'11'11 ' 35 40 + 45 50 l55 67 i 86 11111 '1111 i > < i1'1 * i ■ ■ ■ ■ i 1 ■ ■ • । 60 65 70 75 80 85 90 । ,

95 Abundance #4084: 3-Buten-2-ol, 2-methyl- 7 43 -4 57 . < 4.60 4.80 5.00 5.20 5.40 5000 m/ z 69.10 43.28% 59

27 67 86 53

n/z-> 0 ■■। 20 ■ i ■ I <' I । । -HH । ■ 11 I -HP TIt - 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 1" i' " 111

Abundance #4083:3-Buten-2-ol, 2-methyl- ,14 i ,1 7h 4 60 4.80 5.00 5.20 5.40 43 m/z 59.10 37.50% 5000 ft 1 59 27 31 53 0 1' i ■ ■' ■ i' TTT r137111 - -P ......... *6...... A.. A m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 4.60 4.80 5.00 5.20 5.40

00463.D SCAN508.M Mon Jan 14 10:46:56 2002 Page 4

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