GCMS analysis results for sample AE00319, Jan 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C: \MSDCHEM\1\5973N\02JAN08\319.D Vial: 4 Acq On : 8 Jan 2002 7:56 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508. M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L

Peak Number 4 2-Furanmethanol, tetrahydro... Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

5.01 0.21 ug/L 71044 1,4-Dichlorobenzene-d4 9.72

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 2-Furanmethanol, tetrahydro- (CA... 102 C5H10O2 000097-99-4 59) 2 Butenol, methyl- 86 C5H10O 060766-00-9 (56 3 3-hydroxy-4,4-dimethyl .gamma. B... 130 C6H10O3 052126-90-6 53 4 3-Buten-2-ol, 2-methyl-________________ 86 C5H10O 000115-18-4 50 Abundance Scan 143 (5.006 min): 319.D (-) m/z 43.10 100.00% 43 71

5000 59 39 55 -AA4-M44AA—

m/z-> ob 5 i • ‘ ‘I’’ 10 15 .... । TT 20 25 30 35 40 45 50 55 60 65 70 75 80 85 + 511 — U 84 I ■ * ■ ’ i 90 4.60 m/z 4.80 71.10 5.00 5.20 5.40 98.29% Abundance #9384:2-Furanmethanol, tetrahydro- (CAS) $$ Tetrahydrofur... 7h 43

5000 27 _AN4 V 31 4.60 4.80 5.00 5.20 5.40 m/z 41.10 72.86% 53 37

/z-> 0 1..... ............ Il — i ■11 ■ i " ■ ■ r ■' ■ i TT ............. I1 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 i ’ " • r * • • i •1 ■ ’ i

Abundance #4093: Butenol, methyl- 43 71 _A 4.60 — ... , -A-A— 480 5.00 5.20 5.40 5000 m/z 69.10 46.02% 15 27 31 53 59 J 86 67

m/z-> ob r"■i...... Ial onsiplek Ti 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #26149:3-hydroxy-4,4-dimethyl gamma. Butanolactone $$ Pa... 43 7h 4.60 4.80 5.00 5.20 5.40 m/z 59.00 37.18%

5000

57 31 53 68 0 r 1" i " ■ ■ i .... I........ II 4 — i' " • i • •1 ■ r 1 ■ ■ i -AAAA n/z—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 4.60 4.80 5.00 5.20 5.40

319.D SCAN508.M Wed Jan 09 15:17:57 2002 Page 6

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