DEP GCMS data table, Jan-Feb 2002

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Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004494–000004704

Folder label: “GCMS X 1/30/02 A 2/26/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02FEB26\02084.D Vial: 1 Acq On : 26 Feb 2002 2:44 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 2 6, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 11 4-METHOXY-.BETA.-METHYLCINN... Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T.

22.28 0.12 ug/L 85739 Phenanthrene-dl0 22.63

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 4-METHOXY-.BETA.-METHYLCINNAMIC ... 192 C11H1203 019169-94-9 72 2 l-amino-2-methyl-4-isopropyl-thi... 192 C5H13N4PS 107264-54-0 50 3 N-(2-methylprop-2-enyl)-2-nitrob. .. 192 C10H12N2O2 000000-00-0 47 4 Phenanthrene, 9-methyl- $$ 9-Met... 192 C15H12 000883-20-5 45 Abundance Scan 1675 (22.283 min): 02084.D (-) m/z 192.00 100.00% 192

5000 ..............................................

42 66 82 96 120 146 160 I— 22.00 22.20 22.40 22.60 0 i11 "I 111 u " 1 '111 " 11'1' i' .. .11 TIH m/z 191.00 16.58% m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102588: 4-METHOXY-.BETA.-METHYLCINNAIVIIC ACID $$ 2-Butenoi... 192

108 5000 22.00 2220 22.40 22.60 146 175 m/z 146.10 15.47%

m/z-> O—PPPT ■111 ■ ■ ■ I • • ■ ■ I''1 ■ I ’ ■' ■ I'' I ‘'111 1''' 11'111'' ■ l ■ • ■ > I' ■'' I' ... | 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 U Abundance #101918:1 -amino-2-methyl-4-isopropyI-thiotriazaphospholin... 159 192 AM 22.00 22.20 22.40 22.60 5000 m/ z 95.90 14.68%

144 177

0- TTTTE1"111111111111111111111111/11111111/1111111711117/1157 "‘IT m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102494: N-(2-methylprop-2-enyl)-2-nitrobenzenamine 192 22.00 22.20 22.40 22.60 77 151 m/z 193.00 12.90% 130 93 104 5000 119

177 0 ■ ■ i' ■' ■ i ■ ■ ■ ■ i ■1 ■ ‘ r ■ • ■ i • ■ ■ ■ i T-rp- T-p-T TTT -n-p- 11 ■ ■ ‘' i " '' i ■ ■ " i ■ ‘' i TT-p- m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.00 22.20 22.40 22.60

02084.D HP022102.M Wed Feb 27 08:34:48 2002 Page 13

NYC-WTC_000004601

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NYC-WTC_000004601Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004935

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

3 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999