GCMS analysis results for sample AD31672, Jan 28 2002

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Laboratory report showing GCMS analysis of sample AD31672 including unknown compounds and surrogate recovery data.

NYC-WTC_000050039–000050052

Folder label: “GCMS X 1/3/02 A 1/17/02”

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NYC 9/11 Public Portal Document uOLaLy otaLcIi tompounu Kepor L

Data File : C:\MSDCHEM\1\5973N\02JAN17\31672.D Vial: 7 • Acq On : 17 Jan 2002 7:49 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 17, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 6 4-METHOXY-.BETA.-METHYLCINN... Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 22.28 0.15 ug/L 86693 Phenanthrene-dl0 22.63 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 4-METHOXY-.BETA.-METHYLCINNAMIC ... 192 C11H1203 019169-94-9 72 2 N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 64 3 1,3-Benzodioxole, 4-methoxy-6-(2... 192 C11H12O3 000607-91-0 52 4 N-(2-methylprop-2-enyl)-2-nitrob. .. 192 C10H12N2O2 000000-00-0 46 Abundance Scan 1656 (22.280 min): 31672.D (-) m/z 192.10 100.00% 192

5000

96 146 160 22.00 22.20 22.40 22.60

z—> 0 40 '■! 66 ‘.11 1 TH 120 ■ 11 > । ■ > >«i > i ■ ■ 111 ■ 11 ■ i ■ i [ 11 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 ll— m/z 191.10 16.79% Abundance #102588:4-METHOXY-.BETA.-METHYLCINNAMIC ACID $$ 2-Butenoi... 192

108 * 5000 ' ■■i■■■■i■■■■i ■ ■ ■ ■ i‘ ■ • ■ 22.00 22.20 22.40 22.60 146 175 m/z 96.00 15.41%

m/z—> 0 > ■ I.... t।j,j। j.... j।।. 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance + u #88409: N-perdeuteriobenzylideneaniline 112 ■ 1 1 1 1 1 ■ i 1 1 . I । । I 1 22.00 22.20 22.40 22.60 5000 82 m/z 146.10 14.50% 54 110 30 0 —HP —mmmmtpmmpmt Tpr 11u ■ ‘ i ■ -rrp-rrrpT i 16094

/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102624:1,3-Benzodioxole, 4-methoxy-6-(2-propenyI)- (CAS)... ........... A •’11**I’*I* 1141% 112 22.00 22.20 22.40 22.60 m/z 193.10 14.41% 5000

91 165 103 119 13111____147L_ 177 .I 0- ■ ■ 111।। > 11.11111 ■ । । ■ 1111111 i'|'l 11 ।_____ I . ।.... ।> 11... ।. ।.. ।,... ।..,. ।, MWMr .........M.......... n/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.00 22.20 22.40 22.60

31672.D SCAN508.M Tue Jan 22 08:37:31 2002 Page 8

NYC-WTC_000050050

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GCMS analysis results for sample AD31643, Jan 28 2002 · Box DEP Box 28

NYC-WTC_000049975

Laboratory report showing GCMS analysis of sample AD31643 including unknown compounds and surrogate recovery data.

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