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GCMS analysis results, sample AE12477, June 2002

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Laboratory report showing GCMS analysis results for sample AE12477 including surrogate recovery data on June 10, 2002.

NYC-WTC_000014433–000014459

Folder label: “GCMS X 5/28/02 A 5/29/02

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NYC 9/11 Public Portal Document lenLatively laentinea compound (LSC) summary , Operator ID: McLean Date Acquired: 30 May 2002. 12:45 am - Data File: C:\MSDCHEM\l\DATA\052902\12477.D Name: gc/ms scan 5/28 Mise: Method: C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title: 508 Modified GC/MS scan Library Searched: C:\DATABASE\NIST98.L

--Internal Standard-- TIC Top Hit name RT EstConc Units Response # RT Resp Cone

Acetonitrile, die... 3.52 0.3 ug/L 205417 1 9.90 24094400 40.0 Methylene Chloride 3.73 3.4 ug/L 2073910 1‘ 9.90 24094400 40.0 Pyridine-d5- 3.75 0.8 ug/L 506333 1 9.90 24094400 40.0 Methanethiol 3.76 5.0 ug/L 3003330 1 9.90 24094400 40.0 3-Aminopropionitrile 3.88 0.8 ug/L 459822 1 9.90 24094400 40.0 Perdeuterobenzene 3.90 1.8 ug/L 1114120 1 9.90 24094400 40.0 Methylene Chloride 3.96 0.9 ug/L 568539 1 9.90 24094400 40.0 Acetic acid, chlo... 3.98 2.3 ug/L 1382250 1 9.90 24094400 40.0 l-Buten-3-yne 4.10 1.3 ug/L 779708 1 9.90 24094400 40.0 Methylene Chloride 4.23 1.2 ug/L 732929 1 9.90 24094400 40.0 Methylene Chloride 4.53 0.8 ug/L 477832 1 9.90 24094400 40.0 4H-1,2,4-Triazol- ... 4.69 0.5 ug/L 272588 1 9.90 24094400 40.0 Isocrotonic acid 5.06 0.3 ug/L 151812 1 9.90 24094400 40.0 2-Pentanone, 4-hy... 5.94 1.6 ug/L 956371 1 9.90 24094400 40.0 Cyclopentasiloxan... 12.37 1.4 ug/L 1186380 2 13.39 32794800 40.0 Phenanthrene, 9-m... 22.53 0.2 ug/L 218679 4 22.91 37000100 40.0 Anthracene-d10- 23.06 0.3 ug/L 283820 4 22.91 37000100 40.0 Phthalic acid, di... 31.33 0.3 ug/L 204132 5 30.76 25527400 40.0

12477.D 052202.M Mon Jun 03 11:39:36 2002 Page 22

NYC-WTC_000014459

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NYC-WTC_000014459Source: NYC Law Department, mirrored locally

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