GC/MS results for unknown compounds and surrogates, sample AE10985, May

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\051402\10985.D Vial: 14 Acq On : 15 May 2002 12:06 am Operator: Mclean Sample : 5/10 kb Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ************ ** ******************************************************* Peak Number 11 Hydrazinecarboxamide, 2-(l,... Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T.

35.35 0.28 ug/L 184128 Perylene-dl2 34.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hydrazinecarboxamide, 2- (1,3-dip... 265 C16H15N3O 016983-74-7 10 2 Delachlor 283 C15H22C1NO2 024353-58-0 10 3 Trichothec-9-en-8-one, 12,13-epo... 338 C17H2207 054648-10-1/9 4 .beta.-Chlordene 336 C10H6C16 056534-03-3 9 Abundance Scan 5493 (35.354 min): 10985.D (-5483) (-) m/z 221.10 100. 00% 211 355

49 282

ud... 84 5000 147 191 429 35.00 35.20 35.40 35.60 0 m/z 355.00 89.16% m/z-> 0 50 100 150 200 250 300 350 400 Abundance #87922: Hydrazinecarboxamide, 2-(1,3-diphenyl-2-propenylid... 211

5000 43 77 191 ... IiM, 35.00 35.20 35.40 35.60 104 265 m/z 282.00 62.58%

it 145165 0- 1^ 11,1 1 i 1ii'' । i I ii । 11111 'i ,...................... m/z-> 0 50 100 150 200 250 300 350 400 Abundance #2224: Delachlor 41 1 1 1 35.00 35.20 35.40 35.60 5000 77 132 m/ Z 281.00 61.15%

18 105, 197

00 1 4 50 114 14 1,4162.141226208, 283 n/z-> 100 150 200 250 300 350 400 Abundance #11283: Trichothec-9-en-8-one, 12,13-epoxy-3,7,15-trihydro... 41 173 35.00 35.20 35.40 35.60 83 m/ z 49.00 59.10% 107 5000 135 203223 A/ 2o 290 338

m/z-> 0T 0 50 | 100 150 200 LA 250 300 350 400 ■ 'i' 1 1 ' i 1 ■ 35.00 35.20 35.40 35.60

10985.D 050102.M Thu May 16 14:42:42 2002 Page 14

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