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GCMS analysis results for sample AE11384, May 22 2002

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Laboratory report showing GCMS analysis results for sample AE11384 conducted on May 22, 2002.

NYC-WTC_000025163–000025181

Folder label: “GCMS X 5/15/02 A 5/17/02

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\051702\11383.D Vial : 10 Acq On : 17 May 2002 8:07 pm Operator: Mclean Sample : 5/15 ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 10 Hydrazinecarboxamide, 2-(l,... Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 35.19 0.36 ug/L 324121 Perylene-dl2 34.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual

l Hydrazinecarboxamide, 2-(1,3-dip. .. 265 C16H15N3O 016983-74-7 22 2 2-Propen-1-one, 3-(4-methylpheny . .. 222 C16H140 004224-87-7 10 3 3-Buten-2-one, 4,4-diphenyl- 222 C16H140 000837-66-110 4 Magnesium, bis(2,4-pentanedionat... 222 C10H14MgO4 014024-56/7 10 Abundance Scan 5466 (35.195 min): 11383. D (-5458) (-) m/z 221.10 100.00% 211 1

m/z-> 5000

O-T 49 73 96

-H 147 191

20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 265

'' r 11' i " '' I 295 355

r " ' i1' ■ ■ i'' IT . “y. 34.80 35.00 35.20 35.40 35.60 m/z 207.05 69.73% Abundance #87922: Hydrazinecarboxamide, 2-(1,3-diphenyl-2-propenylid... 205211 UMMMed 77 5000 43 l 1 r ■ r i 1 1 ' ' i ' ■ ' 1 i 1 ' 34.80 35.00 35.20 35.40 35.60 104 265

JM I 128 145 165 180 m/z 355.10 56.94% 246 O-T ||h1 TI‘ — 111111111'1'111111111 ■ ■ i11 1i miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #84905: 2-Propen-1 -one, 3-(4-methylphenyl)-1-phenyl- 207

34.80 35.00 35.20 35.40 35.60 5000 145 m/z 222.10- 54.59% N 105 2 23

/z-> 0420—40+HHlHll 1' p ■ ■ ■ i " 111''' ‘ 111111 ■' ■' i ■' ■ ■ i'' ■11 ‘ 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #87952: 3-Buten-2-one, 4,4-diphenyl- 1tT 211 34.80 35.00 35.20 35.40 35.60 178 m/z 295.00 43.42%

5000

105 43 77 152

m/z-> ol27l4111 -44— 124.126 +44+ । 1uuun—]—um—9uPTp 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 i ■ ■ ■ ■ i - । ■ ' i ■ 1 ■ ■ i ■ ' 34.80 35.00 35.20 35.40 35.60

11383.D 050102 .M Tue May 21 11:55:37 2002 Page 13

NYC-WTC_000025180

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NYC-WTC_000025180Source: NYC Law Department, mirrored locally

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