GCMS scan report for Method 508, April 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\l\DATA\020419\08430.D Vial: 17 Acq On : 19 Apr 2002 11:53 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 15 Cyclopentanecarboxylic acid... Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

44.76 0.47 ug/1 818895 Perylene-dl2 43.16

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentanecarboxylic acid, 1- (... 210 C12H1803 112825-89-5 4 2 3,8-Dioxatricyclo[5.1.0.02,4]oct... 138 C8H10O2 053966-43-1 4 3 3,4-Furandicarboxylic acid 156 C6H405 003387-26-6 4 4 2,4,6-Octatrien-l-ol, 3,7-dimeth... 152 C10H16O 089155-85-1 4 Abundance Scan 7094 (44.760 min): 08430. D (-7083) (-) m/z 40.10 100.00% WWWAWRWWA 43

5000

57 96 109 133147160 282 44.40 44.60 44.80 45.00 81 O+ 1 ‘ 1 1 1 —T— l| Hll j I , IA .......................... .............. ........ , m/z57.10 13.14% m/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #589: Cyclopentanecarboxylic acid, 1-(2-butenyl)-2-oxo-, e... 29 121 A 55

5000 79 137 44.40 44.60 44.80 45.00 94 j m/ z 96.10 13.05% 165 182 01 TTp- +llHh Hl r--।—192 miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #45:3,8-Dioxatricyclo[5.1.0.02,4]octane, 4-ethenyl- 27 41 79 ‘ ‘1 • 44.40 44.60 44.80 45.00 55 m/ z 41.20 9.83% 5000

14 ' 109

nfz—> Ot — 20 J40uLLi 122138 60 80 100 120 140 160 180 200 220 240 260 280 A Abundance #437:3,4-Furandicarboxylic acid 23 45 — 112 m/z 109.10 9.22% 5000 139 156 66 96

•n/z-> 0 pluzihua44 20 40 60 83 ■' i'' 11' ' ' I ‘ ‘' I 1 1 ' ' I ' ‘ ‘11 '1 ‘' I 1 1 1 11 1 1 80 100 120 140 160 180 200 220 240 260 280 ’II 44.40 44.60 44.80 45.00 4 08430.D SCAN020418.M Mon Apr 29 08:29:51 2002 Page 3 0

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