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GCMS blank analysis results for sample AE03184, March 2002

Machine-extracted title · confidence 100%

Laboratory report documenting a GCMS blank test for sample AE03184 conducted on March 6, 2002.

NYC-WTC_000006026–000006044

Folder label: “GCMS X 2/12/02 A 3/01/02

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Scanned page image, NYC-WTC_000006042
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NYC 9/11 Public Portal Document LLDLcLY DedrCI toIpOuIU KCDOL L

Data File : C:\MSDCHEM\l\5973N\02MAR01\0212B.D Vial: 1 Acq On : 1 Mar 2002 10:18 am Operator: Sample : lab blank 2/12 Inst : Instrumen Mise : March 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 12 4-amino-5-bromo-6-methylpyr... Concentration Rank 13

R.T. EstConc Area Relative to ISTD R.T.

23.17 0.03 ug/L 20186 Phenanthrene-dl0 22.63

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 4-amino-5-bromo-6-methylpyrimidine 187 C5H6BrN3 000000-00-0 5 2 2-Chloroethanol 80 C2H5C10 000107-07-3 3 3 Ethanol, 2-chloro- (CAS) $$ Chlo... 80 C2H5C10 000107-07-3 3 4 2-Chloroethanol 80 C2H5C10 000107-07-3 3 Abundance Scan 1754 (23.175 min): 0212B.D (-) m/z 187.10 100.00% 49 187

5000 80 0 17 PMpi ( , Ami l i 22.80 23.00 23.20 23.40 23.60 0+ '1111 H I m r 1'11 ‘'111'' 111112111111111111/17/11111111111111111171’7711 m/z 189.10 94.41% m/z-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 __ Abundance #96248:4-amino-5-bromo-6-methylpyrimidine 189

108 5000 1 I ' ' 1 1 I ' 22.80 23.00 23.20 23.40 23.60 42 54 66 119 m/ z 48.90 90.03% 160 132 147

mte-> 0 " i " " i "111" T’TT "i" 11 ' i" •1111" i" " i ■" TVIPTTTTTT I' " ' I' 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 ...II...... |.. A J |

Abundance #2566:2-Chloroethanol 31 —— — ——— 22.80 23.00 23.20 23.40 23.60 5000 m/ Z 80.05 29.52% 44

61 80 — TTTIWOTg Of I " " 11" ' 1 I "11111'11 I " " I" " r1" I " " i1'" i " " i" mz-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #2568: Ethanol, 2-chloro- (CAS) $$ Chloroethanol $$ 2-Chlo... 1’1’’’’If 31 22.80 23.00 23.20 23.40 23.60 m/z 44.05 6.38%

5000 V U MWwpAN 15

m/z-> 0 ll .44,53 ...... 80..,...... 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 ' i •■•■■■> 1—— 1 ' I * ' * ' I 22.80 23.00 23.20 23.40 23.60

0212B.D HP022102.M Mon Mar 04 12:32:46 2002 Page 14

NYC-WTC_000006042

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NYC-WTC_000006042Source: NYC Law Department, mirrored locally

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