GCMS analysis results for sample AE11380, May 22 2002

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Data File : C:\MSDCHEM\1\DATA\051702\11379.D Vial: 6 Acq On : 17 May 2002 4:51 pm Operator: Mclean Sample : 5/15 ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 5 Phenanthrene-dlO Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 23.11 0.40 ug/L 528786 Phenanthranene-dl0 22.95 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene-dlO 188 C14D10 001517-22-2 91 2 Anthracene-dlO- 188 C14D10 001719-06-8 91/T 3 Selenide, ethyl 1-methyl-1-pente... 188 C8H12Se 025128-48-7 53 4 Cycloheptanone, 4-phenyl-188 C13H16O 067688-28-2 50 Abundance Scan 3409 (23.109 min): 11379.D (-3402) (-) m/z 188.10 100.00% 188

5000

........ / 1 ' i ' 1 1 ■ I r ' ' 1 I 1 1 1 ' I 80 94 22.80 23.00 23.20 23.40 43 57 66 146 160 0 I | ! । । t | I ! ! I | I I I I | 'l I I | t I A | I i । l " I ‘ ' i " " 11" ‘ i" " r 11' r 11 'r1 ■ ril TTT m/z 189.05 15.62% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 188

5000 ....................... ............... 22.80 23.00 23.20 23.40 80 m/Z 184.00 14 .42% 94 160 30 42 52 66 11 108 118 132 146 ,|,| 1701791, | 0 . ..................... I1........ . . I'11'l'' ''I ■','I I I i I | I । i 1 I J I I I I I । । I [ I I I I I I । I i p pHYi I I I [ I I i i | I’Il’lt I I r 11 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-dlO- 188 ........... ........................... .............. 22.80 23.00 23.20 23.40 5000 m/ z 94.10 11.45%

80 94 160 l 30 42 52 7 I 108118 132 146 1 170179 o1I | I ।17 | I | I । i I ] I I I I | I H i । I I i i । I I I I | I । II | I I I I | I I | । [ I I i I | I I I t [ I I I | | I I I | | I I Ir[ i ! i 1 i [ ri i i [ I'Pl mfe-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79821: Selenide, ethyl 1 -methyl-1 -penten-3-ynyl 188 22.80 23.00 23.20 23.40 m/ z 80.10 11.27%

5000 79 159 145 173 91 107 119 131 i /z-> 0 11।।11777 111111111 ■ । > । -l 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 mPm / V 22.80 23.00 23.20 23.40

11379.D 050102.M Mon May 20 15:45:02 2002 Page 8

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