Laboratory report documenting gas chromatography/mass spectrometry analysis of sample AE11413 conducted on May 28, 2002.
NYC-WTC_000025274–000025288Folder label: “GCMS X 5/15/02 A 5/18/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document X wpoul ICpVL
Data File : C:\MSDCHEM\1\DATA\051702\11412.D Vial: 21 Acq On : 18 May 2002 5:54 am Operator: Mclean Sample : 5/15 eh Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e
Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 4 4-Hydroxy-3,5-dimethylcinna... Concentration Rank 4
R.T. EstConc Area Relative to ISTD R.T. 22.58 0.27 ug/L 312261 Phenanthranerie-dl0 22.95 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 4-Hydroxy-3,5-dimethylcinnamic acid 192 C11H12O3 1000132-15-8 59 2 Pyrazine, tetraethyl- 192 C12H20N2 038325-19-8 45 3 2-Propenal, 3-(3,4-dimethoxyphen... 192 C11H1203 004497-40-9 45 4 Phenanthrene, 9-methyl- 192 C15H12 000883-20-5 42 Abundance Scan 3319 (22.580 min): 11412.D (-3310) (-) m/z 192.10 100.00% 192
5000 - 82 96 146 160 22.20 22.40 22.60 22.80 23.00
m/z-> 0 ————————— 49 70 | H > ! | I I । ! | I ! < > | I I ! I [ ! > I I | > I ) , | I I I'l | ! ! ! ! 'J I I I , | , I | | | | I
20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 4 m/z 191.00 22.23% Abundance #81030: 4-Hydroxy-3,5-dimethylcinnamic acid 192
5000 22.20 22.40 22.60 22.80 23.00 89 175 m/z 193.10 14.41% 63 145 45 J 77 105 117 135 | 0 TTTTT+Hl—+44 TTTTTTTTTHHT 163 7 miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80990: Pyrazine, tetraethyl- 192 177 22.20 22.40 22.60 22.80 23.00 5000 m/ z 96.10 13.85% 41 67
m/z-> Abundance 0 am 29 53 81 ,i| 93 107 121 133 149 7 । । i l l | I i i I |‘(11 I I | i i'|'I’| i m i■ |11 rin | t'l'Pi । i Ci'll i r i
20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 #80953: 2-Propenal, 3-(3,4-dimethoxyphenyl)- 163 h I | i ?I u 111+1I’’ ■ 1 1 ■ • ■ । ‘ 1 ‘ ■ i ‘ 192 22.20 22.40 22.60 22.80 23.00 161 m/z 146.10 10.96% 5000 77 91 121 149 177
+ 52 64 103 138
m/z-> 0 - .... 11 , i"' ‘111 HH I'1 " l 0 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.20 22.40 22.60 22.80 23.00
11412.D 050102.M Tue May 21 15:55:47 2002 Page 7
NYC-WTC_000025285
OCR can misread numbers and units. Confirm readings against the page image before using them.
Ranked by indexed similarity. Reasons describe shared subjects and filing context; check the source records.
NYC-WTC_000025289
Laboratory report documenting gas chromatography/mass spectrometry analysis of sample AE11414 conducted on May 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000025332
Fragmented document containing GC/MS data from May 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024100
Laboratory report detailing GCMS analysis of sample AE10897 conducted on May 21, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000025319
Laboratory report documenting gas chromatography/mass spectrometry analysis of sample AE11416 conducted on May 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000025257
Laboratory report showing gas chromatography/mass spectrometry results for sample AE11412 analyzed on May 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000025304
Laboratory report documenting gas chromatography/mass spectrometry analysis of sample AE11415 conducted on May 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023472
Laboratory report showing GC/MS analysis results for sample AE10163 including surrogate recovery data on May 14, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023179
Laboratory report showing GCMS analysis of sample AE09577 conducted on May 14, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023871
Laboratory report showing GC/MS analysis of sample AE10901 with surrogate recovery data for 2,4-DDD.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023156
Laboratory report showing GCMS analysis of sample AE09576 conducted on May 14, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000046094
Gas chromatography-mass spectrometry report for sample AE10815 showing detection of unknown compounds and surrogate recovery.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000046064
Gas chromatography-mass spectrometry report for sample AE10813 showing detection of unknown compounds and surrogate recovery.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
Page similarity is temporarily unavailable or this page has no indexed vector.
Readers open these alongside this record — through an Ask answer, the same folder, or indexed similarity. Not a claim they are about the same event.
NYC-WTC_000025213
Department of Environmental Protection administrative record sheet for World Trade Center site activities dated May 2002.
Filed in the same folder
NYC-WTC_000025214
Document containing GCMS calibration slope information for the period of May 15 to May 18, 2002.
Filed in the same folder
NYC-WTC_000025216
Laboratory report showing GCMS blank analysis for sample AE11410 conducted on May 22, 2002.
Filed in the same folder
NYC-WTC_000025234
Laboratory report documenting GCMS calibration verification for sample AE11410 conducted on May 22, 2002.
Filed in the same folder
NYC-WTC_000025238
GC-MS instrumental data and chromatogram analysis for sample 11410 including compound identification.
Filed in the same folder