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GCMS analysis report sample AE09678, May 23, 2002

Machine-extracted title · confidence 95%

GCMS laboratory report for sample AE09678 detecting unknown compounds and 2,4-DDD on May 23, 2002.

NYC-WTC_000013191–000013216

Folder label: “GCMS X 5/21/02 A 5/21/02

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Scanned page image, NYC-WTC_000013209
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NYC 9/11 Public Portal Document ULDLCLX DedLtii toupOULU KCDOL L

Data File : C:\MSDCHEM\1\DATA\052102\9678.D Vial: 16 Acq On : 22 May 2002 1:33 am Operator: Mclean Sample : re-extract Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 11 Anthracene-dlO- Concentration Rank 16 R.T. EstConc Area Relative to ISTD R.T.

23.07 0.23 ug/L 198813 Phenant hr anene - dl 0 22.91

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Anthracene-dlO- 188 C14D10 001719-06-8 80 2 Phenanthrene-diO 188 C14D10 001517-22-2 64 3 Naphthalene, 2,6-dimethoxy- 188 C12H1202 005486-55-5 9 4 Antipyrine 188 C11H12N2O 000060-80-0 9 Abundance Scan 3402 (23.068 min): 9678.D (-3394) (-) m/z 188.10 100.00% 188

5000

80 94 - 41 51 66 158 22.80 23.00 23.20 23.40 O-pt ...... . .. l'i ।। ■ 11 ■ । . 111 ■ ■ ■ 11111 l ‘ ' I * ’ “ 1 “ “ 11' ‘11 " “ I TI T‘‘T m/z 94.10 19.61% n/z-> 10 20 30 40 50 60 70 80 90 100110120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 188

......... ......................... 5000 22.80 23.00 23.20 23.40 m/z 189.10 19.54% rr 80 94 160 30 ' ‘42 52 66 , n/z-> 0 17 I1 '“i" " i"l ■! “ il|'"'l 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 —10113..132.14617917 il.. Abundance #79827: Phenanthrene-d10 188

22.80 23.00 23.20 23.40 5000 m/z 80.10 18.39%

80 94 160 30 42 52 66 mz-> 1 108118 132 146.1,17917... 0 TumemmmPm—HppHpo •H n p i [ i n 11 *TT1ttt 10 2030405060 70 8090 100110120130140150160170180190 Abundance #79806: Naphthalene, 2,6-dimethoxy- 188 22.80 23.00 23.20 23.40 173 m/z 184.10 14.30% 145 5000 102 28 114 130 15 39 51 63 75 88 0 ‘ I‘*‘‘A‘+++A‘‘‘L+ mmmmh , 157 ’hpmm I‘‘TT .1 Ar l n . m/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 22.80 23.00 23.20 23.40

9678.D 052202.M Wed May 22 11:43:33 2002 Page 14

NYC-WTC_000013209

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NYC-WTC_000013209Source: NYC Law Department, mirrored locally

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