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GCMS calibration data for method 508, May 2 2002

Machine-extracted title · confidence 100%

Calibration data for GCMS analysis of volatile organic compounds recorded on May 2, 2002.

NYC-WTC_000044449–000044450

Folder label: “GCMS X 4/29/02 A 5/1/02

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OCR text

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NYC 9/11 Public Portal Document

Quantitation Report (Not Reviewed)

Data File C:\MSDCHEM\l\DATA\043002\TCMXS.D Vial: 10 Acq On 30 Apr 2002 10:56 pm Operator: Mclean Sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: May 02 09:52:06 2002 Quant Results File: 050102.RES

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Last Update : Thu May 02 09:38:23 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 0.00 152 0 0.00 ug/L -9.95 10) Napthalene-d8 0.00 136 0 0.00 ug/L -13.45 17) Acenapthalene-dlO 0.00 164 0 0.00 ug/L -18.58 29) Phenanthranene-dlO 0.00 188 0 0.00 ug/L -22.97 37) Chrysene-dl2 0.00 240 0 0.00 ug/L -30.86 43) Perylene-dl2 0.00 264 0 0.00 ug/L -34.74

System Monitoring Compounds 2 7) TCMX 20.54 207 693417 0.00 ug/L -0.02 Spiked Amount 10.000 Recovery = 0.00%

Target Compounds Qvalue

(#) = qualifier out of range (m) = manual integration (+) = signals summed TCMXS.D 050102.M Thu May 02 09:52:07 2002 Page 1

NYC-WTC_000044449

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NYC-WTC_000044449Source: NYC Law Department, mirrored locally

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