GCMS analysis results for sample AE06340, May 3 2002

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Gas chromatography-mass spectrometry analysis report for sample AE06340, conducted May 3, 2002, identifying other unknown compounds.

NYC-WTC_000044526–000044540

Folder label: “GCMS X 4/29/02 A 5/1/02”

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Library Search Compound Report Data File C: \MSDCHEM\1\DATA\050102\6340.D Vial : 16 Acq On 1 May 2002 9:55 pm Operator: Mclean Sample re-ext 4/29 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATAJ3ASE\NIST98.L

Peak Number 7 Anthracene-dlO- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

23.11 0.65 ug/L 586244 Phenanthranene-dl0 22.96

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-dlO- 188 C14D10 001719-06-8 72 2 Phenanthrene-dlO 188 C14D10 001517-22-2 59 3 -(4-Tolyl)-3-methyl-pyrazol-5-one 188 C11H12N2O 035496-19-6 38 4 2-Quinolinecarboxaldehyde , 8-hyd... 188 C10H8N2O2 005603-22-5 38 Abundance Scan 3409 (23.109 min): 6340.D (-3403) (-) m/z 188.15 100.00% 188 fl

5000 94 TTT T ‘ I EI ~ l I I I ~ I I I [

m/z-> 43 57 66 80 ! I | I ! ! I [ I I I I | I I ! I | I\ ! ! | I '/ | ! ! I I | I I I I | ! ! I I | I

10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 > I 1 l1 ‘ " I 146 160 TTH .I. 22.80 23.00 23.20 23.40 m/z 94.10 22.78% Abundance #79826: Anthracene-d 10- 188

5000 22.80 23.00 23.20 23.40 m/z 189.10 17.76% 80 94 160 66 17 30 42 52 । . 11 132 108 118 TTt ' i " " i111 ■ r "' i'' " i11 ‘ I | I I I I | I I I I I I I t | I I I I | T I I I | I I I I | I 1461.179179/ Tnr m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 188 1 ' 1 1 ' — ———————— 22.80 23.00 23.20 23.40 5000 m/ z 184.10 13.09%

80 94 160 30 42 52 66 Tpovngi I । । । । । । । | I i । ‘ । I I । । । । I I । । । । l r I ri I | 4—+108,118..132,146—179179l— m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79716: -(4-Tolyl)-3-methyl-pyrazol-5-one 188 22.80 23.00 23.20 23.40 91 m/z 80.05 10.56% 105 5000 119 65 41 51 146| 78 — 1' r 1 " 11'111" ' ■ r111 ‘ r 111 r 1'' i' " 1 r fgo"vugn i i i I1'' 10 1 1 | * i-i । | T> । । । i । i l । i ’ । i । H 3 I I I I I ‘ J I I- I [“I I I I I I I I I [ m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.80 23.00 23.20 23.40

6340.D 050102.M Thu May 02 12:25:17 2002 Page 10

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GCMS analysis results for sample AE06339, May 3 2002 · Box DEP Box 25

NYC-WTC_000044510

Report listing other unknown compounds and surrogate recovery data from GCMS analysis conducted on May 3 2002.

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