GCMS laboratory report for sample AE11908 detecting unknown compounds and 2,4-DDD on June 4, 2002.
NYC-WTC_000013014–000013042Folder label: “GCMS X 5-21-02 A 5-22-02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document__________________________________________ . Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\052202\11908.D Vial: 15 Acq On : 23 May 2002 1:14 am Operator: Mclean Sample : 5/21 ad Inst : Instrumen Mise : Multiplr: 1.00. MS Integration Params: LSCINT.e
Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST9 8.L ********************************************************************* Peak Number 12 Cyclopentasiloxane, decamet... Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T. 12.37 1.44 ug/L 1202730 Napthalene-d8 13.39 Hit# of 5 Tentative ID MW MolForm CAS# Qu. 1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6(90 2 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 50 3 Benzoic acid, 2-[(trimethylsilyl... 282 C13H2203Si2 003789-85-3/38 4 Benzoic acid, 2-[(trimethylsilyl... 282 C13H2203Si2 003789-85-/ 37 Abundance Scan 1582 (12.374 min): 11908.D (-1572) (-) m/z 73.10 100.00% 73
5000 267 355 ....... A........ 45 12.00 12.20 12.40 12.60 12.80 , j 108 133 154 177193 223 251 1 323339 h 0- TIT11011911110020ammaaguT • । * * *• iv “ •14 n “ m/z 267.00 39.59% m/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #115273: Cyclopentasiloxane, decamethyl- 73
5000 267 12.00 12.20 12.40 12.60 12.80 355 m/z 355.10 28.87% 45 0-1 J.n IT TI IT । r 96 115 r. । ,7^ iei, r, ■ 193 nT133149165 , Hi j rF। • i • m’307323339 , rut 251 r’r । n223 28 i' “ ‘a “b1 /z—> 20 40 60 80 1CX) 120 140 160 180 200 220 240 2^) 280 300 320 340 360 Abundance #115315: Cyclopentasiloxane, decamethyl- 73
355 m 12.00 12.20 12.40 12.60 12.80 267 5000 m/z 356.10 10.30%
45 f 0- i "“i“ 191207223 251 “i“"i“i'■ ■11■ “'i• ■ ■ ■ i■■ TIr"it rt■ ।p।ii11।' 4,. ...323339.4., m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #27665: Benzoic acid, 2-[(trimethylsilyl)oxy]-, trimethyls... ’rT T It 73 267 12.00 12.20 12.40 12.60 12.80 m/z 268.00 8.98% 5000
91 135 01. ।।। u r, ""i J ... 47.1 ——41, —115.151 ,. 175 123299,233249 ................... 4—*B—*87p47*an******d*18d*scoddq8dd*18*7**78/*/ n/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 12.00 12.20 12.40 12.60 12.80
11908.D 052202.M Tue May 28 12:15:43 2002 Page 15
NYC-WTC_000013033
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NYC-WTC_000012908
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11903.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012937
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11904.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012794
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11799.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012852
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11901.
2 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012989
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11907.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013496
Laboratory report documenting GCMS analysis of sample AE11928 conducted on June 4, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012823
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11800.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012881
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11902.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013574
Laboratory report documenting GCMS analysis of sample AE11931 conducted on May 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013524
Laboratory report documenting GCMS analysis of sample AE11929 conducted on June 4, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000014578
Laboratory report showing GCMS analysis results for sample AE12534 including surrogate recovery data on June 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000013968
GCMS analysis results for sample AE11603 dated June 4, 2002, documenting unknown compounds and surrogate recovery.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000012748
Department of Environmental Protection record of GCMS results generated in late May 2002.
Filed in the same folder
NYC-WTC_000012749
Administrative log recording sample identification, drip rates, and processing details for a GCMS batch.
Filed in the same folder
NYC-WTC_000012751
Gas chromatography-mass spectrometry blank analysis for sample AE11799 showing results below method reporting limits for semivolatile organic compounds, dated May 28, 2002.
Filed in the same folder
NYC-WTC_000012779
Calibration data for gas chromatography-mass spectrometry analysis of semivolatile organic compounds recorded on May 28, 2002.
Filed in the same folder
NYC-WTC_000012783
Reference standard analysis data for gas chromatography-mass spectrometry testing of semivolatile organic compounds on May 28, 2002.
Filed in the same folder