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GCMS analysis results for sample AE11929, June 2002

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Laboratory report documenting GCMS analysis of sample AE11929 conducted on June 4, 2002.

NYC-WTC_000013524–000013550

Folder label: “GCMS X 5/22/02 A 5/23/02

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\052302\11929.D Vial: 9 Acq On : 23 May 2002 4:29 pm Operator: Mclean Sample : 5/22ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 12 Benzaldehyde Concentration Rank 17 R.T. EstConc Area Relative to ISTD R.T. 8.78 0.21 ug/L 147381 1,4-Dichlorobenzene-d4 9.90 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Benzaldehyde 106 C7H60 000100-52-7/91 2 Benzaldehyde 106 C7H60 000100-52- 91 3 Benzaldehyde 106 C7H60 000100-52- 91 4 Benzaldehyde 106 C7H60 000100-52- 91 Abundance Scan 970 (8.778 min): 11929.D (-965) (-) m/z 105.00 100.00 77 105

51 5000

‘ i ■ • ■ ■ i ■ ‘ i 1 • 1 ■ i ' 1 1 ■ i 1 1 43 — 8.40 8.60 8.80 9.00 9.20 84 0 ' ' | 11 i j i । i i । i । > l+r r i i i । i i m/z 77.10 93.68% nfa-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #115722: Benzaldehyde 77 106

51 5000 8.40 8.60 8.80 9.00 9.20 m/z 106.00 80.89 .... 18 2 0 T-T-i-r-T-T-r-p-T-FrY^^ 63 । 86 ■ ■ ■ l" r ■ l ’’ ‘i ■ ■ ' ■ i ■ ■ ■ ■ i 1 ■ —— 110 nz-> 10 20 30 40 50 60 70 80 90 100 Abundance #119438: Benzaldehyde 77 106 ‘ l ‘ ‘ ' I ‘ ‘ T ■ ■ i ■' ■ ■ । * 51 8.40 8.60 8.80 9.00 9.20 5000 m/z 51.1056.64% ...

27 39

n/z-> 0- m 27. — - 10 50 20 —6098-7 70 30 40 80 90 100 । 4 1 ‘ 1 110 Abundance #115720: Benzaldehyde ■ i ■ ■ ■ ■ i ■ • ■ ■ i ' ■ ■ ■ i ■ ■ ' ■ i ■ 1 77 106 8.40 8.60 8.80 9.00 9.20 m/z 50.10 30.44% 51 5000-

29 39 , O—TT 11161 I 1 24111 34 11 44 1 1 1 1 | ‘ 1 1 1 1 11 1 1 ! 1 56, ,3.,72 86 94 ■ 1 1 i ■ ■ ■ ■ i 1 ■ I ■ i • ■ ' ■ i ■ ‘ i ■ ‘ ■ i ■ 1 /z—> 10 20 30 40 50 60 70 80 90 100 110 8.40 8.60 8.80 9.00 9.20

11929.D 052202.M Wed May 29 09:49:34 2002 Page 15

NYC-WTC_000013543

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NYC-WTC_000013543Source: NYC Law Department, mirrored locally

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