GCMS analysis results for sample AE11926, June 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\052302\11927.D Vial: 7 Acq On : 23 May 2002 2:51 pm Operator: Mclean Sample : 5/22ad Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\052202.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 11 Anthracene-dlO- Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T. 23.07 0.26 ug/L 248336 Phenanthranene-dl0 22.91 Hit# of 5 Tentative ID MW MolForm CAS# Qual 001719-06-8 91 1 Anthracene-dlO- 188 C14D10 2 Phenanthrene-diO 188 C14D10 001517-22-2 47— 3 Benzene, 1-(1-cyclohexen-l-yl)-4... 188 C13H160 020758-60-5 42 4 Pentacyclo[8.4.0.0(3,7).0(4,14).... 188 C14H20 1000099-27-2 36 Abundance Scan 3402 (23.068 min): 11927.D (-3394) (-) m/z 188.05 100.00% 188

5000

40 66 — 80 94 mg 22.80 23.00 23.20 23.40 0------ i ■' “ i “ “ i i ■ ■ “ rn/z 189.10 20.20% n/z-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 188

... 5000 22.80 23.00 23.20 23.40 m/z 94.10 18.02% . 80 94 160 , , _ 17 30 42 52 66 108118 132 146 ,|| 170179i 0-mHm Ttmtn n/z-> 10 2030405060 70 8090 100110120130140150160170180190 Abundance #79827: Phenanthrene-d10 188

22.80 23.00 23.20 23.40 5000 m/z 184.10 14.58%

80 94 160

miz-> 30 42 52 66 0- PmCmmHHpHtTg il 108118 132 146 Totr 17o17lil 10 20 30 40 50 60 70 80 90 100110120 130140150160170180190 ■fTTTT

Abundance। #79791: Benzene, 1 -(1 -cyclohexen-1 -yl)-4-methoxy- . I । *18 I n t i । t v । . 188 22.80 23.00 23.20 23.40 m/z 187.10 13.08% 5000 160

115 129 145 173 41 51 es 77 91 -Hl 102 h | । Hrr lltL, aasparTTT 0- ....................................... /z—> 10 20 30 40 50 60 70 80 90 1(X) 110 120 130 140 150 160 170 180 190 22.80 23.00 23.20 23.40

11927.D 052202.M Wed May 29 09:48:15 2002 Page 14

NYC-WTC_000013494