GCMS analysis results, sample AE09969, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\050602\9969.D Vial: 26 Acq On 7 May 2002 8:03 am Operator: Mclean Sample 4/25 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 9 Benzonitrile, 4-(4-butylcyc... Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

34.96 0.41 ug/L 291004 Perylene-dl2 34.71

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Benzonitrile, 4 -(4-butylcyclohex.. . 241 C17H23N 061204-00-0 9 2 Cyclopropanecarbonitrile, 1-meth... 233 C17H15N 1000145-66-9 9 3 Benzonitrile, 4- (4-pentylcyclohe . . . 255 C18H25N 061204-01-1 9 4 4-(4-Butylcyclohexyl)-benzonitrile 241 C17H23N 1000146-05-2 9 Abundance Scan 5426 (34.960 min): 9969.D (-5424) (-) m/z 264.10 100.00%l 116 . 264 129

73 232 5000 44 ■ । ■ ■ ■ • । > 1 ■ - । ■ ■ ■ ■ । । । । 1 208 34.60 34.80 35.00 35.20 1 1 1 ' 1 1 1 1 ' 1 1 ■ 1 ' 1 i 1 ' 1 1 i ' ' 1 1 1 1 ।1 1 ■ 11 ■'' 11 11 1 ■ । । ■11 ■ ■ m/z 115.90 90.37%| n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #58398: Benzonitrile, 4-(4-butylcyclohexyl)-, trans- 1 6129 41 55 5000 142 ■ । ... . fV i > r। । । ! । । । । । . । r 96 241 34.60 34.80 35.00 35.20 m/z 129.40 83.70% EC 184 | H 120168 |, 198 212 . i 1 1 ■ ■ I1 ' 11I t . । . . t f । । । . . < . । . । . . m/z->_____ 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #52136: Cyclopropanecarbonitrile, 1-methyl-2,2-diphenyl-, (+) 1 6

130 103 34.60 34.80 35.00 35.20 8000 191 206 m/z 132.90 68.52% 165 232

I 218 6000 1 i • 1 1 ■ i ' 1 1 ■ i 1 1 1 1 i 1 1 1 1 i 1 1 1 i 1 1 1 1 I । rn । । । i r । i । ii । r । । ■ । ■ i ■ . /z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #52131: Benzonitrile, 4-(4-pentylcyclohexyl)-, trans- 1 i ' ' 1 ' i 1 il i ' 1 1 ' i ' ' 1 — 1 6129 34.60 34.80 35.00 35.20 m/ z 73.00 61.48% 41 29 55 150 5000 96 255 1. 81 67 184

m/z--> 15 । 1 1 i ‘ 1 1 1 i 1 ■ 20 40 ulL 60 80 100 120 140 160 180 I, 167 198 212 1 '"i ■ ' 1 ‘ 1 1 1 1 1 i rr 1

200 220 240 i 1 '

260 , t , ,171,10, vpl,) l|lllll j 34.60 34.80 35.00 35.20

9969 .D 050102.M Tue May 07 15:48:36 2002 Page 12

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