GCMS analysis results, sample AE09973, May 2002

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Laboratory report for sample AE09973 showing surrogate recovery and unknown compounds from May 9, 2002.

NYC-WTC_000044025–000044054

Folder label: “GCMS X 4/25/02 A 5/7/02”

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Data File C:\MSDCHEM\1\DATA\050602\9973.D Vial: 21 Acq On 7 May 2002 3:59 am Operator: Mclean Sample 4/25 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 17 Benzonitrile, 4-formyl- Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T. 34.93 0.29 ug/L 161242 Perylene-dl2 34.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Benzonitrile, 4-formyl- 131 C8H5NO 000105-07-7 9 2 3,4-Dihydroisoquinoline 131 C9H9N 1000210-20-5 3 lH-Indole-3-ethanamine, .alpha.,... 244 C15H20N2O 1000197-55-8 9 4 Bicine 163 C6H13NO4 000150-25- 1 9 Abundance Scan 5420 (34.925 min): 9973.D (-5419) (-) m/z 86.00 10 . 00% 86 130 207 261 \

J Mon 114

5000 44 281 mw 34.60 34.80 35.00 35.20 1 । 1 ■ ■ ‘ । ■ 1 । 1 1 ' 1 । 1 1 1 1 । 1 > ' । । 1 " ' । ' 1 1 I ' ' 1 ' I ‘ ‘ 1 I 1 ............................ ■ ■ । ■ ■ ■ ■ । । ■ i ■ ■ ■ ■ । I ■ m/z 130.10 89.66% m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #121905: Benzonitrile, 4-formyl- 130 102

5000 76 50 34.60 34.80 35.00 35.20 29 m/z 207.00 85.34% —4 88 it i 63 I T-J-T TTr 117 --pr rr I 1'' । । I ' 1 1 1 1 1 1 1 1 I 1 1 1 1 I 1 1 1 ' l ' apllyMrhyn m/z--> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #58887: 3,4-Dihydroisoquinoline 13 0 1 ’1tt’ 1 I ' 1 1 ' I 1 ' ' ' I 34.60 34.80 35.00 35.20 5000 103 m/z 261.10 81.47% 51 77 39 65 , 89 i . , 4 l. l tph rlr - 116 ------ m/z-> 20 40 60 l80 100 120 140 160 180 200 220 240 260 280 Abundance #58792:1 H-lndole-3-ethanamine, .alpha.,.alpha.-dimethyl-N... 1 4 130 34.60 34.80 35.00 35.20 m/z 129.50 75.43%

5000 86 244 199 T i 46 69

Tl/Z-> L 11.192 20 40 | 142154 170 184 I I I I I I I I I I I I I I I — TTT"T - TH*m——TT

60 80 100 120 140 160 180 200 220 240 260 215 280 ............. .......................... । । । ii ' ।

34.60 34.80 35.00 35.20 । । । । r । । । । । । i i । ■ [

9973.D 050102.M Tue May 07 15:52:04 2002 Page 21

NYC-WTC_000044050

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NYC-WTC_000044050Source: NYC Law Department, mirrored locally

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GCMS analysis results, sample AE09771, May 2002 · Box DEP Box 25

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Laboratory report for sample AE09771 showing surrogate recovery and unknown compounds from May 9, 2002.

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