GCMS analysis results, sample AE09332, May 2002

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Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\050902\9332.D Vial: 22 Acq On : 10 May 2002 9:13 am Operator: Mclean Sample : 5/8 eh Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 7 3,5-Xylyl isocyanide Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T. 34.96 0.27 ug/L 179639 Perylene-dl2 34.70 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3,5-Xylyl isocyanide 131 C9H9N 020600-56-0 9 2 2,3-Dimethylbenzonitrile 131 C9H9N 005724-56-1 9/ 3 Benzonitrile, 3,5-dimethyl- 131 C9H9N 022445-42-79 4 Benzonitrile, 3,4-dimethyl- 131 C9H9N 022884-95-3 9 Abundance Scan 5426 (34.960 min): 9332.D (-5424) (-) m/z 265.10 100.00% 1 6129 265

96 40 281 5000 208 - 34.60 34.80 35.00 35.20 0 i11 ■ ■ i ■ ■ ' 11111111'11 IIt n 1' ।1'1 ■ ।11 T-rp-r m/z 116.00 95.85% miz-> 0 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #52151:3,5-Xylyl isocyanide 1 6 131 5000 34.60 34.80 35.00 35.20 m/z 129.40 94.46% 51 77 103 0 i' 1 1 ■ i ■ ■' ■ i' ■ 11 i 1 ■' 'i ■1 1 ' i1 ' ■ I’’ ----------------- miz-> 0 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #52149: 2,3-Dimethylbenzonitrile t6 131 A M 34.60 34.80 35.00 35.20 5000 m/z 96.10 64.01%

28 51 . 77 103 m/z-> O-TT o 20 —444499.4 । ■11 ) 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #52148: Benzonitrile, 3,5-dimethyl- "ll 1B8 1 T‘ ■ 1 6 34.60 34.80 35.00 35.20 m/Z 130.80 64.01% 131 5000

39 63 77 103 — 0 Ttr 15 1 # I i 4 99 al i ' 1" < । > < > > । । i 1 । । । । । । । । । । । । । । । i । , n/z-> 0 20 40 60 80 100 120 140 160 180 200 220 240 260 280 34.60 34.80 35.00 35.20

9332.D 050102.M Mon May 13 11:43:44 2002 Page 10

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