GCMS analysis results for sample AE10609, May 10 2002

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Laboratory report detailing GC/MS analysis of sample AE10609 including surrogate recovery data in May 2002.

NYC-WTC_000045643–000045661

Folder label: “GCMS X 5/3/02 A 5/7/02”

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\050702\10609.D Vial 12 Acq On 7 May 2002 10:06 pm Operator Mclean Sample 5/3 kb Inst Instrumen Mise Multiplr 1.00 MS Integration Params: LSCINT.e Quant Method C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98.L Peak Number 10 Anthracene-dlO- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

23.11 0.55 ug/L 618474 Phenanthranene-dl0 22.96

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-dlO - 188 C14D10 001719-06-8 94 2 Phenanthrene-dlO 188 C14D10 001517-22-2 91 7 3 Selenide, ethyl 1-methyl-1-pente... 188 C8H12Se 025128-48-7 53 4 Naphthalene, 2,6-dimethoxy-188 C12H1202 005486-55-5 50 Abundance Scan 3409 (23.109 min): 10609.D (-3403) (-) m/z 188.10 100.00% 188

5000 Til | I I I । | I I I । | I | 1 i | | I r i |

p 80 94 22.80 23.00 23.20 23.40

m/z-> ■ ■ ' i ' 1 20 -45-5 40 60 80 100 120 132 146158 — TTTTH 140 160 180 200 1 i ' 1 1 ■ i ■ ■ 220 240 253 1 i m/z 189.10 14.20% Abundance #79826: Anthracene-d10- 188

5000 1 1 । 1 1 T ' | 1 1 1 ■ | 1 1 ' ■ |

22.80 23.00 23.20 23.40 m/Z 184.10 13.67% 88 80 94 1 60 .li T i I ]। 28 i40ph 52 | ? i I J । i' JI |106118 । । i D H । I 3 rd I j rh | ’ 132 146 I > Ipi i t i - i । i I,f | "I । rq i i i i ] i i i T i i i T

m/z->______ 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #79827: Phenanthrene-d10 188 --------- 22.80 23.00 23.20 23.40 5000 m/ z 80.10 12.59%

80 94 160 28 40 52 66 I 108120132 146 1 . . । । । •। ■ 111 । t1, . I11 ■ । rfrmerek———or “I I I 4 1 I I I I I I I I I I I I I I I I" m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #79821: Selenide, ethyl 1 -methyl-1 -penten-3-ynyl ..................................... 1 ■ | 1 1 1 1 T 1 1 m 1 | । 1 ' 1 |-l—r—i-r-1 188 22.80 23.00 23.20 23.40 m/z 94.05 9.59%

5000 79 159 145 173 91 107119131 ,| "I I [ I — — I - I I I I I I—I—I I I 1 r

1 i • 1 ■ 1 i 1 ‘ ' 1 i 1 1 ’ I 1 । | T i 11 ) 1 —1 TI 1 1 I 1 1 1 1 I 1 1 1 1 i 1 ' 1 1 i /z-> 20 40 60 80 100 120 140 160 180 200 220 240 22.80 23.00 23.20 23.40

10609.D 050102.M Thu May 09 09:14:17 2002 Page 13

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