GCMS analysis results for unknown compounds, sample AE10203, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\MSDCHEM\1\DATA\050802\10203.D Vial : 21 Acq On 9 May 2002 7:42 am Operator: Mclean Sample 4/30 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 5 5-Hexen-2-one Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T. 7.73 0.35 ug/L 397846 1,4-Dichlorobenzene-d4 9.94

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 5-Hexen-2-one 98 C6H10O 000109-49-9 10, 2 3-Pyrrolidinol 87 C4H9NO 040499-83-0 8 3 2-Propanone, 1-cyclopropyl- 98 C6H10O 004160-75-2 9 4 5-Hexen-2-one 98 C6H10O 000109-49-9 9 Abundance Scan 791 (7.727 min): 10203.D (-784) (-) m/z 43.10 100.00% 43

5000 58 87 1 1 1 I I 1 1 1 ' I ' 98 7.40 7.60 7.80 8.00 69 m/z-> 01 .......... 37al) । 49, iill. , 10 20 30 40 50 60 70 ' 1 i 1 ' I I , I' 80 90 — 100 m/z 58.05 26.93% Abundance #5001:5-Hexen-2-one 4(3

AAAnyA/Www 5000 f I 1 I I I I T I-1 I I I I I I I 11 I I I T

7.40 7.60 7.80 8.00 55 m/z 87.10 23.12% 15 27 50 60 65 71 77 83 98 0- 11,20..111,32 38,1 ++ T i r-t i °i r i T । i ' I 1 ' 1 1 1 1 m/z--> 10 20 30 40 50 60 70 80 90 100 Abundance #4163: 3-Pyrrolidinol 43 — 1

7.40 7.60 7.80 8.00 5000 m/z 83.00 12.77% 87 57 68 1 o1 1 1 i ■ ' 1 1 i 1 ■ ■ 1 i ' 1 1 1 i , , 52111 , , iI , 77I I 82111 ।111

MM.... I m/z-> Abundance 10 20 30 40

43 50 60 #5149: 2-Propanone, 1 -cyclopropyl- 70 80 !90 100 4 7.40 ' ' I 1 r r । 7.60 7.80 ■ I r । ।

8.00 । । । ।_ । [

m/ z 59.10 12.73% 5000

55 27 98 69 83 m/z-> 0 P......... 10 20 1130...... 1140 L50L 50 , 60 1' I 1 1 177 11 । • i > ■ ■' I I । ■ 70 80 90 100 ................... .. ..................... 7.40 7.60 7.80 8.00 11

10203 .D 050102.M Thu May 09 13:38:08 2002 Page 8

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