GCMS analysis report, sample AE12763, June 2002

NYC 9/11 Public Portal Document Llprary aearen compound Keport Data File C:\MSDCHEM\1\DATA\060602\12763.D vial: 9 Acq On 6 Jun 2002 5:49 pm Operator: McLean Sample 6/3 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integfator) Title : 508 Modified GC/MS scan Library : C: \DATABASE\NIST98 . L

Peak Number 20 n-Hexadecanoic acid Concentration Rank 17

R.T. EstConc Area Relative to ISTD R.T. 25.06 0.41 ug/L 534838 Phenant hr anene - dl 0 22.91 Hit# of 5 Tentative ID MW MolForm CAS# O’

1 n-Hexadecanoic acid 256 C16H3202 000057-10-3 83 2 n-Hexadecanoic acid 256 C16H32O2 000057-10-3 60 3 Pentadecanoic acid 242 C15H30O2 001002-84-2 52 4 n-Decanoic acid 172 C10H20O2 000334-48-5 47 Abundance Scan 3741 (25.060 min): 12763.D (-3732) (-) m/z 149.00 100.00% 43 57 149 73

5000 85 129 ,2 AAA I I I I I 1 I 97 115 213 256

miz-> OTTT 20 1LL ill I UM 120 140 Il 160I TT 40 60 80 100180 200 220 240 X 260 m/z 24.80 25.00 25.20 25.40 57.10 87.18% Abundance #109984: n-Hexadecanoic acid 43 60 73

5000 29 85 97 129 m/z ... a.... 24.80 25.00 25.20 25.40 43.10 84.27% 115 256

miz-> 0-_ 20 1| 40 il In L 60 t" 80 143 157 171 185 199 213 227 241 ha hl rotl) 1 T'‘ *' * ' । ' * 1 ■ । * * ''* । 1 ' । • । ■ 'i ■ • । ■ 100 120 140 160 180 200 220 240 -+ 260 Abundance #6589: n-Hexadecanoic acid 43 60 73 24.80 25.00 25.20 25.40 5000 29 m/z 73.10 79.91% 129 256 85 97 115 143 157 171 185 199.213 227239 0 TT pl m -mne miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #114896: Pentadecanoic acid 1 * i 1 * ■ 1 i .............. 43 60 73 24.80 25.00 25.20 25.40 m/z 60.00 76.85% 5000 129 1 29 87 242 143 IRK 199 98 115 157 171 10 O-T JIM 4 . hu 44 +l . r , 11 , p, .. 213225,,... n/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 24.80 25.00 25.20 25.40

12763.D 060302.M Mon Jun 10 10:29:13 2002 Page 23

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