GCMS sample AE12743 results, June 10 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\MSDCHEM\1\DATA\060602\12761.D vial: 7 Acq On 6 Jun 2002 4:11 pm Operator: McLean Sample 6/3 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan ’" Library : C: \DATABASE\NI ST9 8 . L ********************************************************************* Peak Number 17 2-Propanone, 1,1,1-trichloro- Concentration Rank 19 R.T. EstConc Area Relative to ISTD R.T.

5.93 0.24 ug/L 160928 1,4-dichlorobenzene-d4 9.90

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Propanone, 1,1,1-trichloro- 160 C3H3C130 000918-00-3 40 2 N-Acetylpyrrolidone 127 C6H9NO2 000932-17-24 3 3-Hexadecyloxycarbonyl-5-(2-hydr... 409 C24H45N2O3 1000222-82-8 4 4 Pyrrolidine, 3-methyl- 85 C5H11N 034375-88-8 4 Abundance Scan 486 (5.935 min): 12761 .D (-476) (-) m/ z 43.10 /00.00% 43

5000

■ ‘ i • • • * । ■ ■ • > । 1717/8 |' । 63 85 97 125 5.60 m/z 124.90 5.80 6.00 6.20 0- , 1.t 1, , ■ J. I I. I _ 10.05% n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #3877:2-Propanone, 1,1,1 -trichloro- 43

5000 .. Ill.. 5.60 5.80 6.00 6.20 m/z 84.90 9.12% 15 27 0 ■ i'1, । r'1!-. ’"r 63 83 .97 110.125............ 'K- -i 1 i i | ।" 'i 'i niz->20 40 60 80 100 120 140 160 180 200 220 240 Abundance #7671: N-Acetylpyrrolidone 43 11.8 TI 5.60 5.80 6.00 6.20 5000 m/z 126.90 8.30% 99 127 28 56 86

m/z-> O-r 35 A l, 4 62,1,, -112 20 40 60 100 120 140 160 180 200 220 80 1 ■ ■ i ■ ■ ■ ■ । ■ ■ ■ ■ । ■ i ■ ■ ■ ■ । ‘ । ■1 ■ ■ । 240 Abundance #4219:3-Hexadecyloxycarbonyl-5-(2-hydroxyethyl)-4-methyn... * * i * ■ * * i * • ■ । 1 * * * i * > < * । 43 5.60 5.80 6.00 6.20 m/z 47.00 6.93%

5000 55

I 69 63 O-r ......... .............. . . ........................... •1:4.*4111,11’1+111141+’I n/z—> 20 40 60 80 100 120 140 160 180 200 220 240 5.60 5.80 6.00 6.20

12761.D 060302.M Mon Jun 10 10:25:29 2002 Page 20

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