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GCMS sample AE12743 results, June 10 2002

Machine-extracted title · confidence 90%

Gas chromatography-mass spectrometry analysis report for sample AE12743 detecting unknown compounds and surrogates.

NYC-WTC_000015410–000015438

Folder label: “GCMS X 6/3/02 A 6/6/02”

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NYC 9/11 Public Portal Document Library Searcn Compound Report Data File C:\MSDCHEM\1\DATA\060602\12761.D Vial: 7 Acq On 6 Jun 2002 4:11 pm Operator: McLean Sample 6/3 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan ’5 Library : C: \DATABASE\NIST98 . L

Peak Number 16 Phenol, 6-methyl-2-[(4-morp... Concentration Rank 14

R.T. EstConc Area Relative to ISTD R.T.

5.36 0.32 ug/L 215578 1,4-dichlorobenzene-d4 9.90

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Phenol, 6-methyl-2-[(4-morpholin... 207 C12H17NO2 060460-71-1 9 2 Pyrido[2,3-d]pyrimidine, 4-phenyl- 207 C13H9N3 028732-75-4/5 3 Indole-2-one, 2,3-dihydro-N-hydr . . . 207 C11H13NO3 1000129-52/1 5 4 N-Methyl-1-adamantaneacetamide 207 C13H21NO 1000211-60-4 5 Abundance Scan 389 (5.365 min): 12761.D (-384) (-) Z 35.10 0.00% 35 207 MWNA M M W 5000 49 87 96 500 5.20 5.40 5.60 5.80 I | I I Ji | | I l-i | I I I | । i 1 । l । M — O- ■ i " ■111 ■" i " " i" " r ■ “ i" “ i" " i" ■ ■ i •"' i1 • ■ ■ i " ■ i'" ■ m/z 206.95 84.28% miz-> 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 200 210 Abundance #84739: Phenol, 6-methyl-2-[(4-morpholinyl)methylj- 207 86

5000 121 57 5.00 5.20 5.40 5.60 5.80 . m/z 49.05 27.56% 77 .. 134 149 100 176 .

miz-> 0 TTT** 41 UI . 100 । 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 200 210 thmemmm I 190 U Abundance #84862: Pyrido[2,3-d]pyrimidine, 4-phenyl- 2017

5.00 5.20 5.40 5.60 5.80 50001 m/z 96.10 22.55% 179 77

niz-> O-T 187..73..... . 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 200 210 TTTTT

Abundance #84802: Indole-2-one, 2,3-dihydro-N-hydroxy-4-methoxy-3,3-... 207 5.00 5.20 5.40 5.60 5.80 164 rn/z 87.00 19.25% 5000

147 41 51 63 77 911 104 118 131 176 191

/z-> olryTTTTTytT.^^ - 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 200 210 H 5.00 5.20 5.40 5.60 5.80

12761.D 060302.M Mon Jun 10 10:25:27 2002 Page 19

NYC-WTC_000015433

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NYC-WTC_000015433Source: NYC Law Department, mirrored locally

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