GCMS analysis results, sample AE09331, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\050902\9331.D Vial: 21 Acq On : 10 May 2002 8:24 am Operator: Mclean Sample : 5/8 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator)- Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 3 2-Propanone, 1,1-dichloro- Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T.

3.77 0.32 ug/L 399038 1,4-Dichlorobenzene-d4 9.94

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Propanone, 1,1-dichloro- 126 C3H4C120 000513-88-2 5 2 Ethanol, 2,2-dichloro- 114 C2H4C12O 000598-38-9/9 3 Acetic acid, dichloro-, ethyl ester 156 C4H6C12O2 000535-15-9 9 4 Acetic acid, dichloro-, ethyl ester 156 C4H6C12O2 000535-15-9 9 Abundance Scan 118 (3.773 min): 9331 .D (-114) (-) m/z 43.10 00.00% 43

5000

' ' i ■ ■ ■ ■ i ■ ■ ■ ■ i -

36 51 63 76 83 91 3.40 3.60 3.80 4.00 4.20 0+ ■' i' " ■ i' ■ ‘11 ■ i1 । ’Ml’i IaaIlij JI1.. i1.।।t।।1 ri ।.. m/z 83.00 6.69% m/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #109152:2-Propanone, 1,1-dichloro- 43

/ 5000 r i f' 11 i r r > C] - > । i i-f i- i । Q i 3.40 3.60 3.80 4.00 4.20 m/z 85.00 5.56% 27 — 1 36 50 63 76 83 91 111 126 01 TIITWTTTTTTTTT+ +TTTTT m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #1082: Ethanol, 2,2-dichloro- 31

340 3.60 3.80 4.00 4.20 5000 m/z 84.00 5.52%

miz-> 01 ..... I"'1'1'!1 10 20 30 42 49 61 69 76,83 rU ',|T'''11 >■'1' i " 111''1'' 11 ‘ 40 50 60 70 80 90 96103 114 ■11'' ■ ■ i ■11' i ■' ■' i' ■' ■ i ■' ■11 ■ ■ ■ ■ i ■ ■ 100 110 120 130 140 150 160 " Aw 1___ ”*—KAd Abundance #108006: Acetic acid, dichloro-, ethyl ester 23 3.40 3.60 3.80 4.00 4.20 m/z 63.00 4.17%

5000

15 ,. 48 - 83

tJz-> 0 -H l'| , , 411,57, 65. ! 1.93.190, , 111 , . 123130, 140 , , 154. , . . 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 3.40 3.60 3.80 4.00 4.20

9331.D 050102.M Mon May 13 11:42:35 2002 Page 6

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