GCMS analysis results, Sample AE08264, April 22, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\020417\08264.D Vial: 21 Acq On : 18 Apr 2002 1:56 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 4 2-Propanone, 1,1-dichloro- Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

3.79 0.38 ug/L 452337 1,4-Dichlorobenzene-d4 9.99

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanone, 1,1-dichloro- 126 C3H4C120 000513-88-2 9 2 Ethanol, 2,2-dichloro- 114 C2H4C120 000598-38-9 9 3 Ethanethioic acid 76 C2H40S 000507-09-5 5 4 Acetic acid, dichloro-, ethyl ester 156 C4H6C12O2 000535-15-9 4 Abundance Scan 121 (3 790 min) 08264.D (-110) (-) m/z 43.05 100.00% 43

5000

49 63 76 83 3.40 3.60 3 80 4 00 4 20 36 0 ' 1 1 1 1 1 ' I 1 1 1 ++ 1 ''^r''1 ‘ 1, ■ ।' ■ । ■ । 'l|'' 11 ■ । ■ 111111111111... 111. m/z 82.90 6.42% n/z—> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #109152 2-Propanone, 1,1-dichloro- 43

5000 •< i 'h ' 'O'' । rf ' 1 * 3.40 3.60 3 80 4.00 4 20 m/z 63.00 5.83% 27 , 76 83 91 | ob 49 55 0- 1 1 i 1 ' 1 1 i ' 1 1 r r1 1 rl‘l ' ' ' ' I 63 ' 1 I ' ' 1 ' l '''T' |"' i 1 i | i 1 111 126 Tl/Z--> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #1082 Ethanol, 2,2-dichloro- 31

3.40 3 60 3 80 4 00 4.20 5000 m/ z 49.00 5.14% WA/Wahy 26 0- TITHT 37 43 ■49 11 | । 55 61 70 77. 8388 96 103 114 I | ■ . . , . |‘li. , , , . , 111 . i' .' ■ । . , . , । , , , -r p I ■ I i ■ । i ii I | II Tl/Z--> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #5942: Ethanethioic acid 43 3.40 3.60 3 80 4 00 4.20 m/z 48.00 3.98% 5000

33 > 56 61 76 WwLAA 0 -HH T--m Tl/Z-> 20 30 40 50 60 70 80 90 100 110 120 130 3.40 3 60 3.80 4.00 4 20

08264.D 041702SCAN.M Thu Apr 18 09:52:44 2002 Page 9

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