GCMS analysis report, sample AE12763, June 2002

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Data File C:\MSDCHEM\l\DATA\060602\12763.D Vial: 9 Acq On 6 Jun 2002 5:49 pm Operator: McLean. Sample 6/3 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan . Library- : C:\DATABASE\NIST98.L Peak Number 1 Methane, bromodichloro- Concentration Rank 19 R.T. EstConc Area Relative to ISTD R.T.

3.25 0.36 ug/L 307639 1,4-dichlorobenzene-d4 9.90

Hit# of 5 Tentative ID MW MolForm CAS# Qua

1 Methane, bromodichloro- 162 CHBrC12 000075-27-4( 83 2 Methane, bromodichloro- 162 CHBrC12 000075-27-4 78 3 Chloroform 118 CHC13 000067-66-3 72 4 Chloroform 118 CHC13 000067-66-3 72 Abundance Scan 29 (3.249 min): 12763.D (-24) (-) m/z 82.95 100.00% 83

5000

47 129 3.20 3.30 3.40 3.50 3.60 3.70

mfe-> 0 -H 35 । 1S3 ....... 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 m/z 84.95 71.35% Abundance #33236: Methane, bromodichloro- 83

5000 3.20 3.30 3.40 3.50 3.60 3.70 47 m/z 47.10 19.23% 129

n/z-> O .1103.27, ..... | 93 116 J |, 164 11110-10100-0-0—001" 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #116506: Methane, bromodichloro- 83 3.20 3.30 3.40 3.50 3.60 3.70 5000 m/z 128.90 14,74%

47 129 I9.!. 116 l.l 144 163

m/z-> 13 35 O 1 ■' iri ■11 ■■ ■111 ''i'11 ■ +55,,64,72.4 | i । I I j i | , i j j । j ! fl‘| I 1 ! ! | I"i i i | t i | J | t t i i I'ffl 1 | I I 1

10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #116499: Chloroform 83 3.20 3.30 3.40 3.50 3.60 3.70 m/z 48.10 13.41% "AV 5000

47 MWAO/ 35 0 -mPTTTT .... 701 1 118 111"111" " 111 II"OtuaBTUTr m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 3.20 3.30 3.40 3.50 3.60 3.70

12763.D 060302.M Mon Jun 10 10:28:59 2002 Page 4

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