GCMS analysis results for sample AE09333, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\MSDCHEM\1\DATA\050202\9333.D Vial : 11 Acq On 2 May 2002 7:48 pm Operator: Mclean Sample 4/29 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\l\METHQDS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 2 Acetonitrile, dichloro­ Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 3.61 0.31 ug/L 241963 1,4-Dichlorobenzene-d4 9.94 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetonitrile, dichloro- 109 C2HC12N 003018-12- 2 3,3-Dichloropropyne 108 C3H2C12 1000222-23-9 3 Allyl mercaptan 74 C3H6S 000870-23-5/ 6 4 Thiirane, methyl- 74 C3H6S 001072-43- _______ - 1 9 Abundance Scan 91 (3.614 min): 9333.D (-87) (-) m/z 74.00 100.00% 74

82 5000

35 47 .......... Mal V............... | > । । r jiIIt|iIii।iini|li

88 3.20 3.40 3.60 3.80 4.00 ... ........................ 1 + I । । । । । [ ( । । । । । । । । r m/z 82.00 59.58% 1 1 1 1 1 1 1 1 'I 1 Tn m/z--> 10 20 30 40 50 60 70 80 90 100 110 Abundance #28338: Acetonitrile, dichloro- 74 Ay।1।111।।11 5000 82 3.20 3.40 3.60 3.80 4.00 47 m/ z 84.00 36.09% 35 12 PIT26 I ,ll ll T)B i 62 il , 108 1 1 । । । । । । । । । । । । t । । । "otWoaukonn m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #28312: 3,3-Dichloropropyne 74 I ' 1 1 ' |‘t > ■ I I I I I [ > I I I I I I

3.20 3.40 3.60 3.80 4.00 5000 m/z 76.00 35.55% 38 47 28 || | । 53 60 82 108 m/z-> —————— 10 20 30 40 1 1 I 11 1 1 1 ' 50 60 H 70 80 90 100 110 Abundance #28161: Allyl mercaptan i 1 ' 1 1 i 1 1 1 1 I ' 1 1 1 I 1 1 1 1 I 1 1 41 74 3.20 340 3.60 3.80 4.00 m/z 47.05 21.82% ___ 5000

47 27 33 , T r [ I 1 I I | ) I I I j I I < 111,.11, 53.591.68,1, i । । । m t-] i । । । । [ । । । । । । l I 17 I I I I I Ur I I I L I I I “'I ■ I m/z-> 10 20 30 40 50 60 70 80 90 100 110 3.20 3.40 3.60 3.80 4.00

9333.D 050102.M Mon May 06 13:55:50 2002 Page 6

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