GCMS sample analysis results for AE10606, May 10 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\MSDCHEM\1\DATA\050702\10606.D Vial : 11 Acq On 7 May 2002 9:17 pm Operator: Mclean Sample 5/3 kb Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L Peak Number 1 Ethyl Chloride Concentration Rank 4

R.T. . EstConc Area Relative to ISTD R.T.

3.72 0.35 ug/L 297101 1,4-Dichlorobenzene-d4 9.94

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Ethyl Chloride 64 C2H5C1 000075-00-3 33 86 C4H602 004401-11-0 47/ 2 Ethanone, 1-oxiranyl- 3 2-Butanone, 3-methyl- 86 C5H10O 000563-80-4 4 2,3-Butanedione 86 C4H602 000431-03-8 4 Abundance Scan 109 (3.720 min): 10606.D (-95) (-) m/z 43.10 100.00% 43

5000

49 1 ‘ 1 1 1 ' 1 1 1 1 ‘ 1 "Ott .. 1 .... 1 3.40 3.60 3.80 4.00 " I11" " I ” 111" " I 37 I co 63 TTTTT +HPTTHTTTT I I I | 1 1 । | I ! । > | I I ! ! | ! I 8386 m/z 49.05 21.46% m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #107943: Ethyl Chloride "_PMWApt 23

64 5000 ' 1 ' 1 1 1 1 1 I 1 1 1 ' I ' ' ‘‘011 ' ‘ I 3.40 3.60 3.80 4.00 49 m/z 86.00 13.55% 25 35

m/z-> Abundance n-rr 5 1215 31.438—— ----- _ . I I I I H I I . I I I I I I I 60 67 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 #109927: Ethanone, 1-oxiranyl- 11l’’11111111111 "MwMttp 43 1 ' 1 1 1 ' ' ' I ' ' 1 ' 1 1 1 1 1 I ' ' 1 ' I 3.40 3.60 3.80 4.00 5000 m/ z 84.00 11.71%

71 86

m/z-> I’UII +46,50..565.40.74 82 11 I " '' I 2629 3639 111111 tl11 111111 11 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 i>■ ■ ■ 11•i"■ ■ i "

Abundance #109139: 2-Butanone, 3-methyl- 1 1 1 I ' ' 1 1 I 1 1 '■ 1 I ' ' ' ' I ' ' ' 1 I 43 3.40 3.60 3.80 4.00 m/z 83.00 8.33%

5000

27 39 86

m/z-> i 1 | I 1 11 | । ' 1 1 | r 1t1 31. 24411 475053 31 I । i i i | I i | 57 36.44 I 62 r ।

5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 67 71 75 r i i i । I i i i [ >" | 83 I । |111111,11111 । I । | I । | 2, 3.40 3.60 AMW

3.80 ' l”' A 1 "4 -M i 4.00

10606.D 050102. M Thu May 09 09:11:49 2002 Page 4

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