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GCMS sample analysis results for AE10604, May 10 2002

Machine-extracted title · confidence 100%

Laboratory report detailing GC/MS analysis of sample AE10604 including surrogate recovery data in May 2002.

NYC-WTC_000045595–000045617

Folder label: “GCMS X 5/3/02 A 5/7/02

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\050702\10604.D Vial: 9 Acq On 7 May 2002 7:39 pm Operator: Mclean Sample 5/3 kb Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 1 Ethyl Chloride Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

3.74 0.27 ug/L 229874 1,4-Dichlorobenzene-d4 9.94

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Ethyl Chloride 64 C2H5C1 000075-00-3 28 2 2-Pentanone 86 C5H10O 000107-87-9 9/ 3 Acetyl chloride 78 C2H3C1O 000075-36-5 8 4 Acetyl chloride 78 C2H3C1O 000075-3625 7 Abundance Scan 113 (3 743 min): 10604.D (-103) (-) m/z 43.10 100.00% 43 // 5000

49 ' I 1 I I I I I I I I I I I I I I I I I I I I I

35 20 1 86 3.40 3.60 3.80 4.00 1 r1" i1 ll 11 ‘'11 ‘111 p'" 58 TTTHTTT ■ i I | i । i i | i i i i | I Cl ' [ I i 1’111 m/z 49.10 20.21% m/z-> 0 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance 28 #107943: Ethyl Chloride "woyMontouj 64 5000 ■ ' [i'll ll i l | i । । I | i r ITTDI-1 3.40 3.60 3.80 4.00 49 m/z 42.00 14.59% 35

m/z-> 111 0 mHF 15 24 Th +39—H6I4 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 60 P1" ir 1" i" " r11111111111" i"

Abundance #109359: 2-Pentanone 43 ttTN I 'I I “I I IIUt *-177/1/1/1/1 3.40 3.60 3.80 4.00 5000 m/z 35.10 12.34%

A 27 39 58 71 86 V I ii m/z-> 24 | 31 36 | | ' r "1 r TTIT f 11 u 111111 hi 111" 1111 -TTT 49 53 0 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 + I 63 67 I I। t I I [ I 78 ' > I I I III | I I I [ I I I I I I I I I I I I I I P I l/ Abundance #109117: Acetyl chloride — TT 43 3.40 3.60 3.80 4.00 m/z 86.00 11.97% 15 5000 "M,W/PMWWaiwtsk 63 2 ■ ■ । ■1 ■ ■ । ■ 4.2125,23... ,391 IIIBd10111/1111]anIBannp 49 53 59 | 66 79 83 I I ‘ I I I I I I I I I I I I I I I i I I I I । । । । । । । । > > । । । । । r । । । । i i । । /z-> 0 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 3.40 3.60 3.80 4.00

10604.D 050102.M Thu May 09 09:08:07 2002 Page 4

NYC-WTC_000045603

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NYC-WTC_000045603Source: NYC Law Department, mirrored locally

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