GCMS reference analysis results for volatile organics, June 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File C: \MSDCHEM\1\DATA\060702\12735.D Vial: 11 Acq On 7 Jun 2002 4:43 pm Operator: Sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L Peak Number 12 Ethyl Chloride Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T.

4.65 1.20 ug/L 838582 1,4-dichlorobenzene-d4 9.89

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Ethyl Chloride 64 C2H5C1 000075-00-3 2/ 2 Borane, trifluoro- 68 BF3 007637-07-2 /I 3 1-Propanol, 3-chloro- 94 C3H7C1O 000627-30-5 1 4 2-Chloroethanol 80 C2H5C1O 000107-0773 1 Abundance Scan 267 (4.648 min): 12735.D (-265) (-) m/z 49.10 100.00% 49

5000 86

38 43 4.40 4.60 4.80 5.00 0------ “i “ " i" "i " i' -HHm m/z 84.00 44.63% miz-> 0 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 Abundance #107943: Ethyl Chloride 23

64 5000 4.40 4.60 4.80 5.00 49 m/z 86.00 44.63% 15 35 On‘ss‘1.‘4 mH . . . 1 59fl 11 | i1i11 n 11111111i ■ i11 ■ 1i ] 1i ■ 11i11111i 11 । 11111111111111111111111 n-p >11 TTT + tt

n/z-> 0 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 Abundance #12321: Borane, trifluoro- 49

4.40 4.60 4.80 5.00 5000 m/z 47.10 20.13%

11 19 30 38 68 0 j" • •! • <'' ।. 11111 n 11 n' 11 n । ' ।।।' TWPTTmTTPTTOTTLTTTTTTTTTTTTTT m/z—> 0 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 Abundance #108340:1-Propanol, 3-chloro- 31 4.40 4.60 4.80 5.00 m/z 38.05 8.33% 58 5000

41 V 26

n/z—> 0- 0 m .361 ,11.49..7 , 63 68 1 , 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 _ 76 93 f| »I l hprrr j-i 11 ij 111 > | ii 1111, • > j ■ ■ I > [i > ■ 11111 > । 4.40 4.60 4.80 5.00

12735.D 060302.M Mon Jun 10 11:22:57 2002 Page 15

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