NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\MSDCHEM\1\DATA\050802\10308.D Vial: 11
Acq On 8 May 2002 9:56 pm Operator: Mclean
Sample 5/1 eh Inst : Instrumen
Mise Multiplr: 1.00
MS Integration Params: LSCINT.e
Quant Method : C:\MSDCHEM\l\METHGDS\050102.M (Chemstation Integrator)
Title : 508 Modified GC/MS scan
Library : C:\DATABASE\NIST98.L
Peak Number 9 3,7-Dimethoxyphenothiazine Concentration Rank 5
R.T. EstConc Area Relative to ISTD R.T.
34.99 0.55 ug/L 361002 Perylene-dl2 34.70
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 3,7-Dimethoxyphenothiazine 259 C14H13NO2S1 1000223-22-3 9
2 Glucosamine, 2,3,4,5-tetraacetyl- 347 C14H21NO9 1000127-35-95
3 7,12a-Dimethyl-l,2,3,4,4a,ll,12,. 264 C20H24 075758-27-9 5
4 5H-Naphtho[1,8-bc]thiophen-5-one... 264 C17H120S 010245-6575 5
Abundance Scan 5431 (34.990 min): 10308.D (-5429) (-) m/z 131.50 100.00%
131 259 fl
84
5000 115 281
208
34.60 34.80 35.00 35.20 35.40
O' '. . 44
| । . . I | ■ । I ! | — m/z 259.20 90.38%
'' ।'111111 ■ ■ ।11'11"111
m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340
Abundance #94475: 3,7-Dimethoxyphenothiazine
244209
5000 / _........................
' i 1 1 1 1 i 17 1 ' I ' 1 1 ' i 1 1 ' ' i 1 1
130 34.60 34.80 35.00 35.20 35.40
173 216
201 m/z 264.10 63.78%
63 87 108 —
45
O-4 1.4444—1 r •r‘l i I 146
’mn r i r "p111'1111—
1 I’’’ 11 I ' ' 1 ' I " 'U
m/z->______ 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340
Abundance #8769: Glucosamine, 2,3,4,5-tetraacetyl-
43
-
34.60 34.80 35.00 35.20 35.40
5000 139 m/z 132.90 60.58%
97
259
115
69
m/z->
OU113 prmrkhephho Jil .
40
+4 15411 186211 229 T11 ■ 'I ■i11 " !''1 T’ 111 r"
60 80 100 120 140 160 180 200 220 240 260 280 300 320 340
288 312 330 347
Abundance #95110:7,12a-Dimethyl-1,2,3,4,4a,11,12,12a-octahydrochrysene
1 1 ' 1 1 1 1 1
264 34.60 34.80 35.00 35.20 35.40
m/z 84.00 57.05%
5000 /I
207 /
168 191
153 249 222
Otmmmmmmp li .1, Il',
_ I I
■ ■ । ■ ■ ■ ■ । ।'1111111111' I
'' i'1 ■■ i'1 ■11 TT" 1
Tl/Z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 34.60 34.80 35.00 35.20 35.40
10308.D 050102.M Thu May 09 13:52:32 2002 Page 12
NYC-WTC_000045187
OCR can misread numbers and units. Confirm readings against the page image before using them.