GCMS results for sample AE11425, May 29, 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020521\11425.D Vial: 11 Acq On : 21 May 2002 6:15 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020521.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 6 2-Quinolinecarboxaldehyde, . Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

31.96 0.31 ug/1 33541 Phenanthrene-dl0 31.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Quinolinecarboxaldehyde, 8-hyd. . . 188 C10H8N2O2 005603-22-5 50 2 3-Acetyl-5-methyl-1-phenyl-4,5-d... 231 C12H13N3O2 1000210-22-7 50 3 Naphthalene, 1,7-dimethoxy- 188 C12H1202 005309-18-2 47 4 6-Hydroxy-2-phenyl-3(2H)-pyridaz... 188 C10H8N2O2 1000224-53-6 40 Abundance Scan 4916 (31.964 min): 11425.D (-4908) (-) m/z 188.20 100.00% 188

5000 94 /.................................

143 180 3160 31.80 32.00 32.20 0 ... ..................... .... 335, - ■ ■ ।'1 ■11 ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■11 ■ ■ ■ ■ i ■ ■ ‘ ■ i ■ ■1' ।■11' m/z 94.00 31.00% mlz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #125696:2-Quinolinecarboxaldehyde, 8-hydroxy-, oxime 108

5000 ————————————— 31,60 31,80 32.00 32.20 143 m/z44.10 13.15% 50 AA 64 89I I'Fi115 il'l i At IL 170 O- 1’1’.■ (n, T [*■ Tl,, . i q . . । , । > . . > j\ . । । < i i p-i i i pi i i i ) i

■n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #79690: 3-Acetyl-5-methyl-1 -phenyl-4,5-dihydro-1 H-[1,2,4t... 188 43 31.60 31.80 32.00 32.20 83 231 5000 m/ Z 80.20 10.46% 146 104118 0 । n4d th 111 ■'292217 r » > 11 ri" > 111170 444+ rrd* 1 ...................... i ‘ ■11"1 ■ i ■ ■ ■11" 111' " 1 ’17 ’IT’’’ I n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #79804: Naphthalene, 1,7-dimethoxy- 173108 31.60 31.80 32.00 32.20 m/z 189.15 9.66% 5000 115 145 63 94 130 1 11 ,/............... O- mj n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 31.60 31.80 32.00 32.20

11425.D SCAN020521.M Fri May 24 09:26:47 2002 Page 8

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