GCMS analysis page for sample AE11569, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\020521\11569.D Vial: 22 Acq On : 22 May 2002 5:06 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020521.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ******************************************* * * ************************ Peak Number 1 2-Pentanone, 4-hydroxy-4-me... Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 6.15 16.27 ug/1 1247860 1,4-Dichlorobenzene-d4 11.38 Hit# of 5 Tentative ID MW MolForm CAS# Qual

2-Pentanone, 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 83 2 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 53 3 2-Pentanone, 4 -hydroxy-4-methyl- 116 C6H1202 000123-42-2 42 4 Acenone______ 58 C3H60 000067-64-1 16 Abundance / Scan 523 (6.152 min): 11569.D (-516) (-) m/z 43.05 100.00% 43

5000 59

101 ' ' I ' ‘ 10111,3T I | ■ I l-f T I I I | I . 64 69 83 88 , | 580 6.00 6.20 6.40 01 ........ 38.1 ■ 1 i 1 1 1 1 i 1 1 1 1 i 1 1 1 r i 1 +48 534 I ■ ■ ■ ' I ' । ' ' I 1 ' 1 । I । ‘ ' 1 I' 1 ' ' I ' m/ z 59.10 49.80% n/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #109755: 2-Pentanone, 4-hydroxy-4-methyl- 43

5000 — _____ i 1 ' 1 ' i ' ' ' i ' ' ' ' i ' ' ' ‘ i ' ' 59 580 6.00 6.20 6.40 m/z 58.05 19.52% 15 31 101 Ol 38,, +53+ 26,,1i 1 1. 177/4 1 ' 1111111 I 1 ■ ■ ‘ 1 '■1 1 1 I 83 I *1 । I I ' । 1 I ' 1 1 1 I । miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #5851:2-Pentanone, 4-hydroxy-4-methyl- 43 ■ 1 1 ■ 1 1 । 1 > । 1 । > ' FTI i—r j-i 5 80 6.00 6.20 6.40 5000 m/z 101.10 15.85% 59 101 ol ,1 ,1 T. ............. .. ,3?, 11 ' । ' ' I 1 ' । । | । । i । | । +48 53 '' I ■ ■ ■ ■ । । 67 72 77 । 83 91 96,। । | । । i । । । ' ■ ■ ■ । । । Tl/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #109756: 2-Pentanone, 4-hydroxy-4-methyl- 43 5 80 6.00 6.20 6.40 m/z 41. 10 7.68% 5000 59

0 ......20 26,31.39, —4 S? II/n/Is/IIIIIIIIIIIIIIIII/III 93 101 n/z-> 10 30 40 50 60 70 80 90 100 110 5.80 6.00 6.20 6.40

11569.D SCAN020521.M Fri May 24 09:44:07 2002 Page 3

NYC-WTC_000025598