Laboratory report showing GCMS blank results for volatile organic compounds from sample AE10068 dated May 7-13, 2002.
NYC-WTC_000046117–000046125Folder label: “GCMS X 5/7/02 A 5/14/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\MSDCHEM\1\DATA\020513\0507LB.D Vial: 4 Acq On : 13 May 2002 3:28 pm Operator: Nefliu Sample : 05/07 lab blk Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ******************************************************************** * Peak Number 2 1,2-Phenylene diisothiocyanate Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 31.09 0.29 ug/1 33964 Phenanthrene- dl 0 31.72
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 1,2-Phenylene diisothiocyanate 192 C8H4N2S2 071105-17-4 47 2 Benzene, l-bromo-2-chloro- 190 C6H4BrCl 000694-80-4 47 3 4-Hydroxy-3,5-dimethylcinnamic acid 192 C11H12O3 1000132-15-8 42 4 Bitoscanate 192 C8H4N2S2 004044-65-9 40 Abundance Scan 4767 (31.088 min): 0507LB.D (-4758) (-) m/z 192.05 100.00% 192 A
5000
49 , 70 1 82 96 116 136146 164 | H] i r । 11 > 11 11 > 11 11 11 । r । 11 rTrr 11 |'t i 11 j 11 111 11111 1 i Vrpr 11 r । i H i 111 11 । 11 l~i‘| i । (1111111111 t । t i 11 [ I 111 11 11111 i 30.80 31.00 31.20 31.40 m/z 191.20 25.17% m/z--> 0 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 Abundance #80862: 1,2-Phenylene diisothiocyanate 192
5000 64 l...... 11 1 1 1 ' ‘IZn 30.80 31.00 31.20 31.40 134 75 90 m/z 193.10 24.06% 39 50 , 107 122 4 ■11'" —8.2+ 1+I 4 148 160 ++H rr rh i1! । i 4 I ['I ! I I H’Tr i1H11" ■' I" " r " ■ i" " i n/z->_____ 0 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 Abundance #125825: Benzene, 1 -bromo-2-chloro- 192 111 75 30.80 31.00 31.20 31.40 5000 m/z 146.20 14.98% 50
2 37 1 T+H , । 85 96 m/z-> npm ... 27 1 130141 152 166 177 0 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 11,111" 'T1"111' 11111111111111’" 111111111111111 Trp-r
Abundance #81030: 4-Hydroxy-3,5-dimethylcinnamic acid ■ ' I ' ' ' ' I 1 ' 1 1 I 1 1 1 ' I 192 30.80 31.00 31.20 31.40 m/ z 82.10 12.57% 5000
89 175 _ 63 117 145 T-rp 45 | ill poxsiyenviyouvsyeporsapin 77— +— 10511 TTTTTTT 135 I. 163 I’" n/z-> 0 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 30.80 31.00 31.20 31.40
0507LB.D SCAN020507.M Wed May 15 09:53:30 2002 Page 4
NYC-WTC_000046123
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NYC-WTC_000043749
Laboratory report documenting a method blank analysis for GC/MS testing of volatile organic compounds from May 2002.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024748
Reference document describing Method 509 procedures for laboratory analysis, dated February 14, 1992.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024427
Record of sample preparation parameters including drip rates and volumes for GCMS analysis conducted in mid-May 2002.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024534
Laboratory report showing blank test results for GCMS analysis of sample AE11282 conducted between May 13 and May 16, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000025499
Laboratory report showing non-detect levels for 15 volatile organic compounds in a GCMS method blank processed on May 17-21, 2002.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000022495
Technical log detailing gas chromatography mass spectrometry method parameters and calibration settings from May 2002.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048602
Laboratory blank analysis results confirming absence of contamination in GCMS testing for volatile organic compounds.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048085
Laboratory report showing non-detect results for volatile organic compounds in a GCMS blank run (Sample AE08323) from April to May 2002.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024927
Laboratory report documenting GCMS analysis of sample AE10301 conducted on May 10, 2002, including surrogate recovery data.
1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000025568
GCMS analysis report for sample AE11567 showing unknown compounds and surrogate recovery data from May 29, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024484
Laboratory report documenting GCMS analysis of sample AE11153 conducted on May 22, 2002, including surrogate recovery data.
1 shared non-person entities · 1 shared topics · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024907
Laboratory report documenting GCMS analysis of sample AE10247 conducted on May 28, 2002, including surrogate recovery data.
1 shared non-person entities · 1 shared topics · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000046112
Department of Environmental Protection GCMS analysis record for the World Trade Center site dated May 7-14 2002.
Filed in the same folder
NYC-WTC_000046113
Header page for GCMS Method 06 analysis records from DEP Box 25 dated May 7-14, 2002.
Filed in the same folder
NYC-WTC_000046126
Laboratory report showing GCMS calibration results for volatile organic compounds from sample AE10068 dated May 7-13, 2002.
Filed in the same folder
NYC-WTC_000046130
Laboratory report showing GCMS reference standard results for volatile organic compounds from sample AE10068 dated May 7-13, 2002.
Filed in the same folder
NYC-WTC_000046135
Calibration table data for GCMS analysis of volatile organic compounds dated May 13-14, 2002.
Filed in the same folder