GCMS calibration table data, May 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\MSDCHEM\l\DATA\020513\0507REF2.D Vial: 8 Acq On : 13 May 2002 7:26 pm Operator: Nefliu Sample : 05/07 ref Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e Quant Time: May 14 15:51:01 2002 Quant Results File: SCAN020507.RE

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Last Update : Thu May 09 09:21:01 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN1

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.38 152 441486 40.00 ug/1 -0.01 10) Naphthalene-d8 16.53 136 1633864 40.00 ug/1 -0.04 17) Acenaphthene-diO 24.46 164 862248 40.00 ug/1 -0.02 30) Phenanthrene-diO 31.72 188 1481185 40.00 ug/1 -0.02 38) Chrysene-dl2 39.94 240 1216415 40.00 ug/1 -0.05 44) Perylene-dl2 43.16 264 741086 40.00 ug/1 -0.02

System Monitoring Compounds 2 7) TCMX 27.54 207 62104 9.02 ug/1 -0.04 Spiked Amount 10.000 Recovery = 90.20%

Target Compounds Qvalue 2) N-nitrosodimethylamine 4.00 74 45923m 6.52 ug/1 3) bis(2-Chloroethyl)ether 10.65 93 265198 15.53 ug/1 98 4) 1.3-Dichlorbenzene 11.12 146 197125 13.83 ug/1 97 5) 1,4-Dichlorobenzene 11.43 146 206635 13.28 ug/1 99 6) 1,2-Dichlorobenzene 11.96 146 202807 15.01 ug/1 99 7) 2,2‘oxybis(1-Chloropropane 12.78 45 453093m 16.61 ug/1 8) N-Nitroso-di-n-propylamine 13.26 43 207240 16.96 ug/1 97 9) Hexachloroethane 13.26 119 77923 11.54 ug/1 97 11) Nitrobenzene 13.67 77 321190 16.38 ug/1 98 12) Isophorone 14.78 82 652390 19.09 ug/1 98 13) bis(2-Chloroethoxy) methan 16.02 93 337485 16.63 ug/1 98 14) 1,2,4-Trichlorobenzene 16.38 180 179011 15.27 ug/1 99 15) Naphthalene 16.62 128 701153 17.12 ug/1 99 16) Hexachlorobutadiene 17.40 225 96839 14.23 ug/1 90 18) 2-Chloronaphthalene 21.93 162 388332 18.92 ug/1 98 19) Acenaphthylene 23.75 152 639593 15.97 ug/1 99 20) Dimethyl phthalate 23.84 163 481957 18.00 ug/1 98 21) 2,6-Dinitrotoluene 23.95 77 45547 19.75 ug/1 # 84 22) Acenaphthene 24.60 153 413290 17.80 ug/1 97 23) 2,4-Dinitrotoluene 25.73 165 100557 16.31 ug/1 94 24) Fluorene 27.00 166 505524 18.93 ug/1 99 25) Diethyl phthalate 27.22 149 531800 19.75 ug/1 97 26) 4-Chlorophenyl-phenylether 27.34 204 232962 17.61 ug/1 96 28) N-Nitrosodiphenylamine 27.94 168 155098 17.82 ug/1 99 29) Azobenzene 28.02 77 676768 16.45 ug/1 99 31) Hexachlorobenzene 29.60 284 144880 18.54 ug/1 99 32) 4-Bromophenyl-phenylether 29.71 248 133764 17.49 ug/1 96 33) Phenanthrene 31.81 178 683640 18.15 ug/1 99 34) Anthracene 32.04 178 616065 16.15 ug/1 99 35) Di-n-butylphthalate 34.81 149 876155 18.59 ug/1 99

(#) = qualifier out of range (m) = manual integration 0507REF2.D SCAN020507.M Tue May 14 15:51:33 2002 Page 1

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