GCMS calibration table data, May 2002

NYC 9/11 Public Portal Document

f Quantitation Report (QT Reviewed)

Data File : C:\MSDCHEM\l\DATA\020513\0507REF2.D Vial: 8 Acq On : 13 May 2002 7:26 pm Operator: Nefliu Sample : 05/07 ref Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e Quant Time: May 14 15:51:01 2002 Quant Results File: SCAN020507.RE

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Last Update : Thu May 09 09:21:01 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN1

Compound R.T. Qlon Response Cone Unit Qvalue

36) Fluoranthene 36.05 202 772568 18.20 ug/1 99 39) Pyrene 36.66 202 802396 18.86 ug/1 99 40) Buthylbenzylphthalate 38.93 149 365644 17.87 ug/1 95 41) Benz(a)anthracene 39.92 228 658650 17.46 ug/1 98 42) Chrysene 40.00 228 663687 18.69 ug/1 100 43) Bis(2-ethylhexyl)phthalate 40.52 149 467184 17.93 ug/1 94 45) Di-n-Octyl phthalate 42.03 149 626424 15.52 ug/1 98 46) Benzo(b)fluoranthene 42.37 252 515961 17.95 ug/1 100 47) Benzo(k)fluoranthene 42.44 252 552517 18.79 ug/1 99 48) Benzo(a)pyrene 43.02 252 345750 12.55 ug/1 99 49) Indeno(1,2,3-cd)pyrene 45.22 276 250995 12.31 ug/1 95 50) Dibenz(a,h)anthracene 45.32 278 287774 14.89 ug/1 99 51) Benzo(ghi)perylene 45.77 276 301560 15.44 ug/1 98

(#) = qualifier out of range (m) = manual integration (+) = signals summed 0507REF2.D SCANO20507.M Tue May 14 15:51:33 2002 Page 2

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