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GCMS reference standard results, May 2002

Machine-extracted title · confidence 100%

Laboratory record of reference standard analysis for volatile organic compounds using GCMS methods from May 13 to May 15, 2002.

NYC-WTC_000024441–000024449

Folder label: “GCMS X 5/13/02 A 5/16/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File : C:\MSDCHEM\1\DATA\020515\0513REF4.D Vial: 8 Acq On : 15 May 2002 6:44 pm Operator: Nefliu Sample : 05/13 ref Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e Quant Time: May 16 14:50:47 2002 Quant Results File: SCAN020507.RE

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Last Update : Thu May 16 14:49:15 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN1

Compound R.T. Qlon Response Cone Unit Qvalue

36) Fluoranthene 36.05 202 676364 16.82 ug/1 96 39) Pyrene 36.66 202 696845 17.51 ug/1 97 4 0) Buthylbenzylphthalate 38.93 149 311757 16.28 ug/1 96 41) Benz(a)anthracene 39.92 228 578939 16.41 ug/1 98 42) Chrysene 39.99 228 583403 17.56 ug/1 99 43) Bis(2-ethylhexyl)phthalate 40.52 149 533055 21.87 ug/1 94 45) Di-n-Octyl phthalate 42.03 149 522287 13.92 ug/1 99 46) Benzo(b)fluoranthene 42.37 252 449940 16.84 ug/1 99 47) Benzo(k)fluoranthene 42.43 252 483717 17.70 ug/1 97 48) Benzo(a)pyrene 43.02 252 330755 12.92 ug/1 94 49) Indeno(1,2,3-cd)pyrene 45.22 276 205272 10.83 ug/1 97 50) Dibenz(a,h)anthracene 45.32 278 235465 13.11 ug/1 99 51) Benzo(ghi)perylene 45.76 276 257477 14.18 ug/1 99

(#) = qualifier out of range (m) = manual integration (+) = signals summed 0513REF4.D SCAN020507.M Thu May 16 14:51:20 2002 Page 2

NYC-WTC_000024448

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NYC-WTC_000024448Source: NYC Law Department, mirrored locally

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