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GCMS calibration results for sample AE10241, May 2002

Machine-extracted title · confidence 95%

Laboratory report of GCMS calibration data for sample AE10241 conducted between May 14 and May 16, 2002.

NYC-WTC_000024762–000024769

Folder label: “GCMS X 5/14/02 A 5/17/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File : C:\MSDCHEM\1\DATA\020516\0514REF2.D Vial: 9 Acq On : 16 May 2002 5:16 pm Operator: Nefliu Sample : 05/14 ref Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Time: May 17 10:37:19 2002 Quant Results File: SCAN020507.RE

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Last Update : Thu May 16 14:49:15 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN1

Compound R.T. Qlon Response Cone Unit Qvalue

36) Fluoranthene 36.05 202 559696 18.07 ug/1 96 3 9) Pyrene 36.66 202 586703 19.42 ug/1 97 40) Buthylbenzylphthalate 38.93 149 255871 17.61 ug/1 98 41) Benz(a)anthracene 39.92 228 469737 17.54 ug/1 100 42) Chrysene 39.99 228 463072 18.37 ug/1 99 43) Bis(2-ethylhexyl)phthalate 40.52 149 317806 17.18 ug/1 97 45) Di-n-Octyl phthalate 42.03 149 405577 14.63 ug/1 98 46) Benzo(b)fluoranthene 42.37 252 356071 18.03 ug/1 99 47) Benzo(k)fluoranthene 42.43 252 382334 18.92 ug/1 95 48) Benzo(a)pyrene 43.02 252 265464 14.03 ug/1 100 49) Indeno(1,2,3-cd)pyrene 45.22 276 165282 11.80 ug/1 96 50) Dibenz(a,h)anthracene 45.32 278 183313 13.80 ug/1 99 51) Benzo(ghi)perylene 45.77 276 217438 16.20 ug/1 94

(#) = qualifier out of range (m) = manual integration (+) = signals summed 0514REF2.D SCAN020507.M Fri May 17 10:37:49 2002 Page 2

NYC-WTC_000024765

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NYC-WTC_000024765Source: NYC Law Department, mirrored locally

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