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GCMS calibration verification data for sample AE11424, May 2002

Machine-extracted title · confidence 95%

Calibration verification report listing response factors for target compounds in sample AE11424 analyzed May 17-21, 2002.

NYC-WTC_000022508–000022515

Folder label: “GCMS X 5/17/12 A 5/21/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed) Data File : C:\MSDCHEM\1\DATA\020521\0517REF2.D Vial: 6 Acq On : 21 May 2002 1:20 pm Operator: Nefliu Sample : 052/17 ref kb Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e Quant Time: May 24 09:16:29 2002 Quant Results File: SCAN020521.RE Quant Method : C:\MSDCHEM\1\METHODS\SCAN020521.M (RTE Integrator) Title : Method 508 GC/MS Scan Last Update : Tue May 21 08:15:50 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN1

Compound R.T. Qlon Response Cone Unit Qvalue 36) Fluoranthene 36.05 202 595012 14.83 ug/1 99 3 9) Pyrene 36.66 202 635627 16.60 ug/1 98 40) Buthylbenzylphthalate 38.93 149 267420 14.75 ug/1 97 41) Benz(a)anthracene 39.91 228 497455 14.86 ug/1 98 42) Chrysene 39.99 228 516937 16.34 ug/1 98 43) Bis(2-ethylhexyl)phthalate 40.52 149 323048 14.35 ug/1 99 45) Di-n-Octyl phthalate 42.03 149 384392 11.43 ug/1 99 46) Benzo(b)fluoranthene 42.37 252 366745m 15.42 ug/1 47) Benzo(k)fluoranthene 42.43 252 406623 15.50 ug/1 100 4 8) Benzo(a)pyrene 43.02 252 239015 10.45 ug/1 96 49) Indeno(1,2,3-cd)pyrene 45.22 276 135642m 9.30 ug/1 50) Dibenz(a,h)anthracene 45.32 278 158571 11.34 ug/1 98 51) Benzo(ghi)perylene 45.76 276 193687 13.37 ug/1 94

(#) = qualifier out of range (m) = manual integration (+) = signals summed 0517REF2.D SCAN020521.M Fri May 24 09:17:44 2002 Page 2

NYC-WTC_000022511

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NYC-WTC_000022511Source: NYC Law Department, mirrored locally

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