GCMS calibration verification data for sample AE11424, May 2002

Quantitation Report (QT Reviewed) Data File : C:\MSDCHEM\l\DATA\020521\0517REF2.D Vial: 6 Acq On : 21 May 2002 1:20 pm Operator: Nefliu Sample : 052/17 ref kb Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Time: May 24 9:17 2002 Quant Results File: SCAN020521.RES Method : C:\MSDCHEM\1\METHODS\SCAN020521.M (RTE Integrator) Title : Method 508 GC/MS Scan Last Update : Fri May 24 09:17:31 2002 Response via : Initial Calibration Abundance TIC: 0517REF2.D 2200000

2000000 of

1800000

1600000 z o zs o r 1400000 1 i t 2 tg I § E& S C)

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1200000 1 l o Q.

! o i s 9 ut 1000000 6 I H 15 I i I % 2 12<0 i = I SaB I 1 l I> 2 2 800000 3 a g‘ 11 i | 8 2 III Sai 2 S 8 g 5 ■ I a8 if g$

e |r 8 8 0

600000 fill 8zg 8 3® 1 8g i 5 ©

§ 1 §g 2 it C CD E X 400000 i I 24 • g• iz Qe N* % 8 o Sr r 6 § 63 § X & 8 § t 2 I 8% I a 11 a8 fl O o Q co 200000 2 1 E CXI LO t CXI o Q o Time-> 0 —

4.00 6.00 • T1 । - I 8.00 10.00 12.00 Ul —L 14.00 . 16.00 18.00 AA . 20.00 22.00 ।' ‘ ‘ । ■ 11 JU U. TTTTTT J 1 1 ■ 1 i ' 24.00 26.00 28.00 30.00 32.00 34.00 36.00 38.00 40.00 42.00 44.00 46.00 f ■H-r CXI o o o o oX I o Q 0517REF2.D SCAN020521.M Fri May 24 09:17:45 2002 Page 3 I o d > o 7 > 7