GCMS reference results for sample AE11282, May 2002

Quantitation Report (QT Reviewed) Data File : C:\MSDCHEM\1\DATA\O2O516\O513REF1.D Vial: 6 Acq On : 16 May 2002 2:19 pm Operator: Nefliu Sample : 05/13 ref Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Time: May 17 10:30 2002 Quant Results File: SCAN020507.RES Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Last Update : Thu May 16 14:49:15 2002 Response via : Initial Calibration Abundance TIC: 0513REF1.D 1800000

2 TH 1600000 9

1400000 i o z8 o‘

8.o I8 1200000 £& C

Z £ § 2 £ c 1f a 5 1000000 2 2o 8 s I fs £ g fS 588 0

0 8, ! 88 2d g 8 I Ka 1 2o

i 800000 2 2 22 o § s& 2 W

£82 Ig 2 1 8 3 I m 8 2 600000 [li l 2 ffgl Zo 2 2 i 2 I (XC 1 E

2 8 6 |

28 1 5 g 1 JaF ia I I $ 0

! I 8352 9 ' I Q

8 8 4 E S0 fl C CD E 400000 [ g r. Z8 Q* - SI g N N 8 Eesl w. s § 2 a & I |i O o 200000 Q LO co L t o Q 0 1 ..... 1 ■i i Jl A I ‘ r ' 1 1 1 TIT TIIT- 1 1 1 । 1 1 ' 1 1 o O O o 9 Time-> 4.00 6.00 8.00 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00 26.00 28.00 30.00 32.00 34.00 36.00 38.00 40.00 42.00 44.00 46.00 O o O I Q

oo 0513REF1.D SCAN020507.M Fri May 17 10:31:14 2002 Page 3 3 d> 2 > 7