GCMS calibration verification data for sample AE11424, May 2002

Quantitation Report (QT Reviewed) Data File : C:\MSDCHEM\1\DATA\020521\0517REF1.D Vial: 5 Acq On : 21 May 2002 12:21 pm Operator: Nefliu Sample : 052/17 ref kb Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Time: May 24 9:16 2002 Quant Results File: SCAN020521.RES Method : C:\MSDCHEM\1\METHODS\SCAN020521.M (RTE Integrator) Title : Method 508 GC/MS Scan Last Update : Tue May 21 08:15:50 2002 Response via : Initial Calibration Abundance TIC:0517REF1.D 2600000

2400000 2 2200000

2000000 G Ji o

1800000 1s fs s 2 g I 2 £w I 1600000

1400000 § 5 a 8 g Q.

8c O

I 8n f .0s1 28 5 a I i a t §8 g I

I I 1200000 2d 8 $

J 2 2 5 § ( - C D 1000000 2 75 o &I I9 a m S inI a tIt 5 g s83,£ & 11 2 s §g8 Eca $85 2 ft’ o £ & 2 I 38

I 2 ia & 2 800000 Hit it § 28 i 5 |g 8555 -8 a I !

i &Q

C O 600000 2 f 002 9 2019 % 2 y. z8 * Q 93 w% 2 I§ 8N i c a S| E 5 400000 S 6E I o o N X

. 11 I O o Q LO 200000 c co LO t o Q o Time-> 0 ‘‘III ~ r1 T-r-rr 4.00 6.00 8.00 -4 10.00 12.00 14.00 U ----- ’ f 1 1 1 1 1 I TTTdumm 16.00 18.00 20.00 22.00 24.00 26.00 28.00 30.00 32.00 T—mm IIn/tm 1 Tur - 34.00 36.00 38.00 40.00 42.00 44.00 N 46.00 CXI CXI o o o o o I o Q — oo 0517REF1.D SCAN020521.M Fri May 24 09:16:24 2002 Page 3 sd > > 7 7