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GCMS calibration verification data for sample AE11424, May 2002

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Calibration verification report listing response factors for target compounds in sample AE11424 analyzed May 17-21, 2002.

NYC-WTC_000022508–000022515

Folder label: “GCMS X 5/17/12 A 5/21/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed) Data File : C:\MSDCHEM\l\DATA\020521\0517REFl.D Vial: 5 Acq On : 21 May 2002 12:21 pm Operator: Nefliu Sample : 052/17 ref kb Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e Quant Time: May 24 09:15:41 2002 Quant Results File: SCAN020521.RE Quant Method : C:\MSDCHEM\1\METHODS\SCAN020521.M (RTE Integrator) Title : Method 508 GC/MS Scan Last Update : Tue May 21 08:15:50 2002 Response via : Initial’Calibration DataAcq Meth : 508SCAN1

Compound R.T. Qlon Response Cone Unit Qvalue 36) Fluoranthene 36.05 202 849443 17.96 ug/1 97 3 9) Pyrene 36.66 202 892929 19.23 ug/1 97 40) Buthylbenzylphthalate 38.93 149 391580 17.81 ug/1 94 41) Benz(a)anthracene 39.92 228 700656 17.26 ug/1 99 42) Chrysene 40.00 228 699492 18.23 ug/1 99 43) Bis(2-ethylhexyl)phthalate 40.52 149 482937 17.70 ug/1 99 45) Di-n-Octyl phthalate 42.03 149 628470 15.36 ug/1 98 46) Benzo(b)fluoranthene 42.38 252 529685m 18.31 ug/1 47) Benzo(k)fluoranthene 42.43 252 555656 17.42 ug/1 95 48) Benzo(a)pyrene 43.02 252 354878 12.76 ug/1 99 49) Indeno(1,2,3-cd)pyrene 45.22 276 215099 12.12 ug/1 98 50) Dibenz(a,h)anthracene 45.32 278 238368 14.02 ug/1 97 51) Benzo(ghi)perylene 45.77 276 277293 15.74 ug/1 99

(#) = qualifier out of range (m) = manual integration (+) = signals summed 0517REF1.D SCAN020521.M Fri May 24 09:16:23 2002 Page 2

NYC-WTC_000022514

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NYC-WTC_000022514Source: NYC Law Department, mirrored locally

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