GCMS reference standard results for sample AE10812, May 2002

Quantitation Report (QT Reviewed) Data File : C:\MSDCHEM\l\DATA\020521\0517REF3.D Vial: 7 Acq On : 21 May 2002 2:19 pm Operator: Nefliu Sample : 052/17 ref ad Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e Quant Time: May 24 9:18 2002 Quant Results File: SCAN020521.RES Method : C:\MSDCHEM\1\METHODS\SCAN020521.M (RTE Integrator) Title : Method 508 GC/MS Scan Last Update : Fri May 24 09:17:56 2002 Response via : Initial Calibration Abundance TIC: 0517REF3.D

2600000

2400000

2200000

5 3 I!> 2000000- G 8 6 a« g EI c 1800000 6 2 f o

I C

Z & 2 I8 1600000- 1 1 2 g2 g i8 £ 1400000 1 I& 8 0 2

s1 o i 88 £ S 1 1200000 2 5 0 S 9 I O 8 2 D 5 3 6 go I ft e o i 1 I m 6& w m

rJ 1000000 yal88 ?g 2 11! 8 L

IJ I Pii 48 O 29 2 g § 2 | £ O

1 s

s Is 800000 5 8 9N 18 E 1 & c

C CD E 600000

400000 I I 2 CC :Q &24 i 2 in N

&8 N & o% 0. Q

2 N 4 cm" 3 I I I

g§&s 15 O o Q O co 200000 t LO o LO ____ — — CXI 1BT --4 U ■ 11 1 1 1 Q 0MP| I I I -I. | I Jr-. ....| I I I' I [ 1 — o o I W I I I I TId o Time-> 4.00 6.00 8.00 10.00 12.00 14.00 16.00 18.00 20.00 22.00 24.00 26.00 28.00 30.00 32.00 34.00 36.00 38.00 40.00 42.00 44.00 46.00 o o o 1 0- O 0517REF3.D SCAN020521.M Fri May 24 09:18:37 2002 Page 3 o Id O > > 7 7