GCMS reference results for sample AE11282, May 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\MSDCHEM\1\DATA\020516\0513REF2.D Vial: 7 Acq On : 16 May 2002 3:18 pm Operator: Nefliu Sample : 05/13 ref Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e Quant Time: May 17 10:31:31 2002 Quant Results File: SCAN020507.RE

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Last Update : Thu May 16 14:49:15 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN1

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.38 152 290563 40.00 ug/1 -0.01 10) Naphthalene-d8 16.53 136 1100810 40.00 ug/1 -0.04 17) Acenaphthene-diO 24.46 164 593509 40.00 ug/1 -0.02 30) Phenanthrene-diO 31.72 188 1004214 40.00 ug/1 -0.02 38) Chrysene-dl2 39.94 240 761099 40.00 ug/1 -0.05 44) Perylene-dl2 43.15 264 448773 40.00 ug/1 -0.03

System Monitoring Compounds 27) TCMX 27.56 207 159555 33.65 ug/1 -0.02 Spiked Amount 40.000 Recovery 84.13%

Target Compounds Qvalue 2) N-nitrosodimethylamine 4.00 74 28124m 6.07 ug/1 3) bis(2-Chloroethyl)ether 10.65 93 186157 16.56 ug/1 97 4) 1.3-Dichlorbenzene 11.11 146 153632 16.38 ug/1 99 5) 1,4-Dichlorobenzene 11.43 146 161230 15.74 ug/1 96 6) 1,2-Dichlorobenzene 11.95 146 151784 17.07 ug/1 97 7) 2,2'oxybis(1-Chloropropane 12.78 45 313625m 17.46 ug/1 8) N-Nitroso-di-n-propylamine 13.25 43 148495 18.47 ug/1 97 9) Hexachloroethane 13.26 119 60697 13.66 ug/1 90 11) Nitrobenzene 13.67 77 224132 16.96 ug/1 97 12) Isophorone 14.78 82 456072 19.81 ug/1 99 13) bis(2-Chloroethoxy) methan 16.02 93 235647 17.23 ug/1 97 14) 1,2,4-Trichlorobenzene 16.38 180 130834 16.57 ug/1 97 15) Naphthalene 16.62 128 508986 18.45 ug/1 100 16) Hexachlorobutadiene 17.39 225 74666 16.29 ug/1 96 18) 2-Chloronaphthalene 21.93 162 280294 19.84 ug/1 96 19) Acenaphthylene 23.75 152 459009 16.65 ug/1 99 20) Dimethyl phthalate 23.84 163 343368 18.63 ug/1 98 21) 2,6-Dinitrotoluene 23.96 77 29366 18.50 ug/1 91 22) Acenaphthene 24.59 153 301341 18.85 ug/1 98 23) 2,4-Dinitrotoluene 25.73 165 70937 16.71 ug/1 95 24) Fluorene 27.00 166 354874 19.30 ug/1 100 ■ 25) Diethyl phthalate 27.22 149 383159 20.67 ug/1 100 26) 4-Chlorophenyl-phenylether 27.35 204 167436 18.39 ug/1 94 28) N-Nitrosodiphenylamine 27.94 168 121224 20.24 ug/1 97 29) Azobenzene 28.03 77 484513 17.11 ug/1 99 31) Hexachlorobenzene 29.59 284 102208 19.30 ug/1 99 32) 4-Bromophenyl-phenylether 29.71 248 96763 18.66 ug/1 92 33) Phenanthrene 31.81 178 488235 19.12 ug/1 99 34) Anthracene 32.04 178 444711 17.19 ug/1 98 35) Di-n-butylphthalate 34.81 149 613858 19.21 ug/1 99

(#) = qualifier out of range (m) = manual integration 0513REF2.D SCAN020507.M Fri May 17 10:34:15 2002 Page 1

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