GCMS reference standard results for sample AE10812, May 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\MSDCHEM\1\DATA\020521\0517REF4.D Vial: 8 Acq On : 21 May 2002 3:18 pm Operator: Nefliu Sample : 052/17 ref ad Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e Quant Time: May 24 09:18:42 2002 Quant Results File: SCAN020521.RE

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020521.M (RTE Integrator) Title : Method 508 GC/MS Scan Last Update : Fri May 24 09:17:56 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN1

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.38 152 455808 40.00 ug/1 -0.01 10) Naphthalene-d8 16.54 136 1702072 40.00 ug/1 -0.03 17) Acenaphthene-diO 24.46 164 906433 40.00 ug/1 -0.02 30) Phenanthrene-diO 31.72 188 1552062 40.00 ug/1 -0.02 38) Chrysene-dl2 39.94 240 1210903 40.00 ug/1 -0.05 44) Perylene-dl2 43.15 264 709359 40.00 ug/1 -0.03

System Monitoring Compounds 27) TCMX 27.56 207 240188 33.04 ug/1 -0.04 Spiked Amount 40.000 Recovery 82.60%

Target Compounds Qvalue 2) N-nitrosodimethylamine 3.98 74 44623m 6.31 ug/1 3) bis(2-Chloroethyl)ether 10.65 93 292508 16.55 ug/1 99 4) 1.3-Dichlorbenzene 11.11 146 221157 14.77 ug/1 96 5) 1,4-Dichlorobenzene 11.43 146 231393 14.13 ug/1 97 6) 1,2-Dichlorobenzene 11.96 146 225488 15.82 ug/1 98 7) 2,2'oxybis(1-Chloropropane 12.78 45 492125m 17.57 ug/1 8) N-Nitroso-di-n-propylamine 13.25 43 223342 17.53 ug/1 99 9) Hexachloroethane 13.25 119 81991 11.44 ug/1 92 11) Nitrobenzene 13.67 77 349427 16.57 ug/1 99 12) Isophorone 14.78 82 681417 18.85 ug/1 100 13) bis(2-Chloroethoxy) methan 16.02 93 358910 16.76 ug/1 97 14) 1,2,4-Trichlorobenzene 16.38 180 193480 15.22 ug/1 92 15) Naphthalene 16.62 128 765165 17.57 ug/1 99 16) Hexachlorobutadiene 17.40 225 89636 11.97 ug/1 92 18) 2-Chloronaphthalene 21.92 162 420317 18.98 ug/1 100 19) Acenaphthylene 23.75 152 686365 16.17 ug/1 98 20) Dimethyl phthalate 23.84 163 518135 17.96 ug/1 97 21) 2,6-Dinitrotoluene 23.96 77 49218m 18.59 ug/1 2 2) Acenaphthene 24.60 153 450347 17.92 ug/1 95 23) 2,4-Dinitrotoluene 25.73 165 113041 16.93 ug/1 93 24) Fluorene 27.00 166 534362 18.49 ug/1 99 25) Diethyl phthalate 27.22 149 574487 19.69 ug/1 96 26) 4-Chlorophenyl-phenylether 27.35 204 255308 17.73 ug/1 97 28) N-Nitrosodiphenylamine 27.94 168 174137 18.00 ug/1 99 29) Azobenzene 28.03 77 743066 16.78 ug/1 98 31) Hexachlorobenzene 29.60 284 151034 18.03 ug/1 99 32) 4-Bromophenyl-phenylether 29.71 248 146373 17.60 ug/1 88 3 3) Phenanthrene 31.82 178 725882 17.98 ug/1 99 34) Anthracene 32.04 178 657989 16.17 ug/1 98 35) Di-n-butylphthalate 34.81 149 950238 19.00 ug/1 99

(#) = qualifier out of range (m) = manual integration 0517REF4.D SCAN020521.M Fri May 24 09:19:13 2002 Page 1

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