GCMS reference results for sample AE11282, May 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\MSDCHEM\1\DATA\020516\0513REF1.D Vial: 6 Acq On : 16 May 2002 2:19 pm Operator: Nefliu Sample : 05/13 ref Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e Quant Time: May 17 10:30:17 2002 Quant Results File: SCAN020507.RE

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Last Update : Thu May 16 14:49:15 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN1

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.37 152 314623 40.00 ug/1 -0.02 10) Naphthalene-d8 16.53 136 1189661 40.00 ug/1 -0.04 17) Acenaphthene-diO 24.46 164 638222 40.00 ug/1 -0.02 30) Phenanthrene-diO 31.72 188 1091203 40.00 ug/1 -0.02 38) Chrysene-dl2 39.94 240 878133 40.00 ug/1 -0.04 44) Perylene-dl2 43.15 264 517689 40.00 ug/1 -0.03

System Monitoring Compounds 27) TCMX 27.56 207 179727 35.25 ug/1 -0.02 Spiked Amount 40.000 Recovery 88.13%

Target Compounds Qvalue 2) N-nitrosodimethylamine 3.96 74 36796m 7.34 ug/1 3) bis(2-Chloroethyl)ether 10.65 93 211022 17.34 ug/1 95 4) 1.3-Dichlorbenzene 11.11 146 170197 16.75 ug/1 94 5) 1,4-Dichlorobenzene 11.43 146 174876 15.77 ug/1 97 6) 1,2-Dichlorobenzene 11.95 146 170157 17.67 ug/1 98 7) 2,2'oxybis(1-Chloropropane 12.78 45 348795m 17.94 ug/1 8) N-Nitroso-di-n-propylamine 13.25 43 163407 18.77 ug/1 96 9) Hexachloroethane 13.25 119 66583 13.84 ug/1 95 11) Nitrobenzene 13.67 77 248730 17.42 ug/1 96 12) Isophorone 14.78 82 497128 19.98 ug/1 97 13) bis(2-Chloroethoxy) methan 16.02 93 266632 18.04 ug/1 98 14) 1,2,4-Trichlorobenzene 16.39 180 147904 17.33 ug/1 99 15) Naphthalene 16.62 128 564504 18.93 ug/1 99 16) Hexachlorobutadiene 17.39 225 82506 16.66 ug/1 93 18) 2-Chloronaphthalene 21.92 162 303223 19.96 ug/1 98 19) Acenaphthylene 23.75 152 506279 17.07 ug/1 97 20) Dimethyl phthalate 23.84 163 376190 18.98 ug/1 98 21) 2,6-Dinitrotoluene 23.95 77 33068 19.37 ug/1 98 22) Acenaphthene 24.59 153 326326 18.99 ug/1 96 23) 2,4-Dinitrotoluene 25.74 165 75183 16.47 ug/1 88 24) Fluorene 27.00 166 390564 19.76 ug/1 100 25) Diethyl phthalate 27.22 149 410620 20.60 ug/1 98 26) 4-Chlorophenyl-phenylether 27.35 204 183176 18.71 ug/1 98 28) N-Nitrosodiphenylamine 27.94 168 131964 20.49 ug/1 99 29) Azobenzene 28.02 77 541078 17.77 ug/1 98 31) Hexachlorobenzene 29.60 284 112466 19.54 ug/1 99 32) 4-Bromophenyl-phenylether 29.71 248 108092 19.19 ug/1 94 33) Phenanthrene 31.82 178 528867 19.06 ug/1 99 34) Anthracene 32.04 178 494111 17.58 ug/1 99 35) Di-n-butylphthalate 34.81 149 671724 19.34 ug/1 100

(#) = qualifier out of range (m) = manual integration 0513REF1.D SCAN020507.M Fri May 17 10:31:14 2002 Page 1

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